1,2-Diiodo-3-methoxybenzene

Base Information

Chemical Name:1,2-Diiodo-3-methoxybenzene
CAS No.:98991-10-7
Molecular Formula:C7H6I2O
Molecular Weight:359.933
Hs Code.:
DSSTox Substance ID:DTXSID201310137

Synonyms:1,2-diiodo-3-methoxybenzene;98991-10-7;SCHEMBL4136425;VFFUMIVINUVMHO-UHFFFAOYSA-N;DTXSID201310137

Suppliers and Price of 1,2-Diiodo-3-methoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,2-Diiodo-3-methoxybenzene

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:359.85081
Heavy Atom Count:10
Complexity:108

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=CC=C1)I)I

Technology Process of 1,2-Diiodo-3-methoxybenzene

There total 3 articles about 1,2-Diiodo-3-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 197243-48-4
2-iodo-3-nitrophenol

: 74-88-4
methyl iodide

: 98991-10-7
3-methoxy-1,2-diiodobenzene

Guidance literature:: 2-iodo-3-nitrophenol; methyl iodide;

With iron(III) chloride; hydrazine; Further stages.;
DOI:10.1021/ol0255054

Reference yield:

: 98991-08-3
2-iodo-1-methoxy-3-nitrobenzene

: 98991-10-7
3-methoxy-1,2-diiodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / N₂H₄*H₂O, FeCl₃*6H₂O, C / methanol / 47 h / Heating

2: 1.) NaNO₂, aq. HCl, 2.) KI / 1.) H₂O, 5 deg C, 50 min, 2.) H₂O, 80 deg C, 2 h

With hydrogenchloride; iron(III) chloride; hydrazine hydrate; potassium iodide; sodium nitrite; In methanol;
DOI:10.1021/jo00225a020

Reference yield:

: 98991-09-4
2-iodo-3-methoxyphenylamine

: 98991-10-7
3-methoxy-1,2-diiodobenzene

Guidance literature:: With hydrogenchloride; potassium iodide; sodium nitrite; Yield given. Multistep reaction; 1.) H₂O, 5 deg C, 50 min, 2.) H₂O, 80 deg C, 2 h;
DOI:10.1021/jo00225a020