4-(2,6-Dichlorobenzoyl)toluene

Base Information

Chemical Name:4-(2,6-Dichlorobenzoyl)toluene
CAS No.:99508-49-3
Molecular Formula:C14H10Cl2O
Molecular Weight:265.139
Hs Code.:
DSSTox Substance ID:DTXSID10545831
Wikidata:Q82423456

Synonyms:4-(2,6-dichlorobenzoyl)toluene;99508-49-3;SCHEMBL7266220;DTXSID10545831;SAXPLHZLZBSMQE-UHFFFAOYSA-N;(2,6-Dichloro-phenyl)-p-tolyl-methanone;(2,6-Dichlorophenyl)(4-methylphenyl)methanone

Suppliers and Price of 4-(2,6-Dichlorobenzoyl)toluene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 4-(2,6-Dichlorobenzoyl)toluene

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:264.0108703
Heavy Atom Count:17
Complexity:261

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)C2=C(C=CC=C2Cl)Cl

Technology Process of 4-(2,6-Dichlorobenzoyl)toluene

There total 4 articles about 4-(2,6-Dichlorobenzoyl)toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 20082-66-0
trimethyl(2,6-dichlorophenyl)silicium

: 100-07-2
4-methoxy-benzoyl chloride

: 99508-49-3
2,6-dichloro-4'-methylbenzophenone

Guidance literature:: With aluminium trichloride; In dichloromethane; for 48h; Heating;
DOI:10.1016/S0040-4020(01)80238-6

Reference yield:

: 108-88-3,15644-74-3,16713-13-6
toluene

: 4659-45-4
2,6-Dichlorobenzoyl chloride

: 99508-49-3
2,6-dichloro-4'-methylbenzophenone

Guidance literature:: With aluminium trichloride; at 85 ℃; for 15h;

Reference yield:

: 541-73-1
1,3-Dichlorobenzene

: 99508-49-3
2,6-dichloro-4'-methylbenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 1.) n-BuLi/TEMEDA / tetrahydrofuran; hexane / 19 h / -75 - 20 °C

2: 60 percent / AlCl₃ / CH₂Cl₂ / 48 h / Heating

With n-butyllithium; aluminium trichloride; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/S0040-4020(01)80238-6