(2,6-Dichlorophenyl)trimethylsilane

Base Information

Chemical Name:(2,6-Dichlorophenyl)trimethylsilane
CAS No.:20082-66-0
Molecular Formula:C9H12Cl2Si
Molecular Weight:219.186
Hs Code.:
European Community (EC) Number:659-901-8
Nikkaji Number:J2.268.799I

Synonyms:20082-66-0;1,3-Dichloro-2-(trimethylsilyl)-benzene;(2,6-DICHLOROPHENYL)TRIMETHYLSILANE;SCHEMBL12188521;2,6-Dichlorophenyltrimethylsilane;AKOS024338624

Suppliers and Price of (2,6-Dichlorophenyl)trimethylsilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (2,6-Dichlorophenyl)trimethylsilane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:218.0085323
Heavy Atom Count:12
Complexity:143

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C1=C(C=CC=C1Cl)Cl

Technology Process of (2,6-Dichlorophenyl)trimethylsilane

There total 4 articles about (2,6-Dichlorophenyl)trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 75-77-4
chloro-trimethyl-silane

: 541-73-1
1,3-Dichlorobenzene

: 20082-66-0
trimethyl(2,6-dichlorophenyl)silicium

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -75 - 20 ℃; for 19h;
DOI:10.1016/S0040-4020(01)80238-6

Reference yield: 29.0%

: 876070-70-1
(2,6-dichloro-3-iodophenyl)trimethylsilane

: 1026390-15-7
2,4,3'-trichloro-3,2'-bis-trimethylsilanyl-biphenyl

: 2,4,4'-trichloro-3,3'-bis-trimethylsilanyl-biphenyl

: 20082-66-0
trimethyl(2,6-dichlorophenyl)silicium

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; pentane; at -100 - -75 ℃; for 1.5h;
DOI:10.1002/ejoc.200500553

Reference yield:

: 29898-32-6
2,4-dichloro-1-iodo-benzene

: 20082-66-0
trimethyl(2,6-dichlorophenyl)silicium

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / BuLi / hexane; tetrahydrofuran / -75 °C

2: 29 percent / tBuLi / tetrahydrofuran; pentane / 1.5 h / -100 - -75 °C

With n-butyllithium; tert.-butyl lithium; In tetrahydrofuran; hexane; pentane;
DOI:10.1002/ejoc.200500553