5-Methyl-2-methylthiopyridine

Base Information

Chemical Name:5-Methyl-2-methylthiopyridine
CAS No.:51933-75-6
Molecular Formula:C7H9NS
Molecular Weight:139.22
Hs Code.:
DSSTox Substance ID:DTXSID301303395
Nikkaji Number:J1.333.044A
Mol file:51933-75-6.mol

Synonyms:5-Methyl-2-methylthiopyridine;51933-75-6;5-methyl-2-methylsulfanylpyridine;5-Methyl-2-(methylthio)pyridine;5-methyl-2-methylsulfanyl-pyridine;5-METHYL-2-(METHYLSULFANYL)PYRIDINE;SCHEMBL485398;2-(Methylthio)-5-methylpyridine;DTXSID301303395;BCA93375;MFCD22628233;CS-0195705;5-Methyl-2-(methylthio)pyridine, AldrichCPR;E92505

Suppliers and Price of 5-Methyl-2-methylthiopyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AOBChem
5-Methyl-2-methylthiopyridine 95%
100g
$ 3456.00

Total 7 raw suppliers

Chemical Property of 5-Methyl-2-methylthiopyridine

Chemical Property:

Boiling Point:228.4 °C at 760 mmHg
Flash Point:91.9 °C
PSA：38.19000
Density:1.07 g/cm³
LogP:2.11190
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:139.04557046
Heavy Atom Count:9
Complexity:85

Purity/Quality:

99% ^*data from raw suppliers

5-Methyl-2-methylthiopyridine 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 22-36
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CN=C(C=C1)SC

Technology Process of 5-Methyl-2-methylthiopyridine

There total 5 articles about 5-Methyl-2-methylthiopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-99-6
3-Methylpyridine

: 624-92-0
Dimethyldisulphide

: 51933-75-6
5-methyl-2-(methylsulfanyl)pyridine

Guidance literature:: 3-Methylpyridine; With n-butyllithium; lithium 2-(dimethylamino)ethanolate; In hexane; at 0 ℃; for 1h;

Dimethyldisulphide; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Further stages.;
DOI:10.1039/b001690j

Reference yield: 80.0%

: 3510-66-5
2-Bromo-5-methylpyridine

: 867-44-7,147895-43-0
S-Methylisothiourea sulfate

: 51933-75-6
5-methyl-2-(methylsulfanyl)pyridine

Guidance literature:: With caesium carbonate; In dimethyl sulfoxide; at 80 ℃; for 6h;
DOI:10.1039/c8ob01758a

Reference yield:

: 6457-37-0
(3-methylpyridine)BF₃

: 624-92-0
Dimethyldisulphide

: 51933-75-6
5-methyl-2-(methylsulfanyl)pyridine

Guidance literature:: (3-methylpyridine)BF₃; With n-butyllithium; diisopropylamine; In diethyl ether; at -78 ℃; for 0.416667h;

Dimethyldisulphide; In diethyl ether; at -78 - 20 ℃;

With water; In diethyl ether; regioselective reaction;
DOI:10.1002/ejoc.201101592