Technology Process of 7-Methoxy-6-methyl-1-indanone
There total 1 articles about 7-Methoxy-6-methyl-1-indanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
Heating;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: cerium(III) chloride / tetrahydrofuran / 0 - 20 °C
2.1: HCl / methanol / 4 h / Heating
3.1: 0.36 g / hydrogen / Pd/C / 10 h / 760 Torr
4.1: 90 percent / acetic acid; NBS / 2 h / 85 °C
5.1: n-BuLi / tetrahydrofuran / 0.5 h / -75 °C
5.2: tetrahydrofuran / 24 h / 20 °C
5.3: NaOH / H2O / 1 h
6.1: 0.30 g / Cs2CO3 / Pd(PPh3)4 / dimethylformamide; H2O / 2 h / 120 °C
7.1: BBr3 / CH2Cl2 / 4 h / 15 °C
With
hydrogenchloride; N-Bromosuccinimide; n-butyllithium; cerium(III) chloride; hydrogen; boron tribromide; caesium carbonate; acetic acid;
palladium on activated charcoal; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
6.1: Suzuki coupling;
DOI:10.1021/ol052956q
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: cerium(III) chloride / tetrahydrofuran / 0 - 20 °C
2.1: HCl / methanol / 4 h / Heating
3.1: 0.36 g / hydrogen / Pd/C / 10 h / 760 Torr
4.1: 90 percent / acetic acid; NBS / 2 h / 85 °C
5.1: n-BuLi / tetrahydrofuran / 0.5 h / -75 °C
5.2: tetrahydrofuran / 24 h / 20 °C
5.3: NaOH / H2O / 1 h
6.1: 0.30 g / Cs2CO3 / Pd(PPh3)4 / dimethylformamide; H2O / 2 h / 120 °C
With
hydrogenchloride; N-Bromosuccinimide; n-butyllithium; cerium(III) chloride; hydrogen; caesium carbonate; acetic acid;
palladium on activated charcoal; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
6.1: Suzuki coupling;
DOI:10.1021/ol052956q
