3-(6-Oxo-1,6-dihydro-3-pyridazinyl)benzonitrile, 97%

Base Information

• Chemical Name: 3-(6-Oxo-1,6-dihydro-3-pyridazinyl)benzonitrile, 97%
• CAS No.: 52240-08-1
• Molecular Formula: C11H7N3O
• Molecular Weight: 197.196
• Mol file: 52240-08-1.mol

Synonyms:3-(6-oxo-1,6-dihydropyridazin-3-yl)benzonitrile;3-(6-Oxo-1,6-dihydro-3-pyridazinyl)benzonitrile;Benzonitrile, 3-(1,6-dihydro-6-oxo-3-pyridazinyl)-;3-(6-Oxo-1,6-dihydro-3-pyridazinyl)benzonitrile,97%;3-(6-oxo-1,6-dihydropyridazin-3-yl)benzonitrile(WXC04974)

Chemical Property of 3-(6-Oxo-1,6-dihydro-3-pyridazinyl)benzonitrile, 97%

Chemical Property:

• PSA: 69.54000
• LogP: 1.30858

Purity/Quality:

99%, ^*data from raw suppliers

3-(6-OXO-1,6-DIHYDRO-PYRIDAZIN-3-YL)-BENZONITRILE 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(6-Oxo-1,6-dihydro-3-pyridazinyl)benzonitrile, 97%

There total 3 articles about 3-(6-Oxo-1,6-dihydro-3-pyridazinyl)benzonitrile, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-acethylbenzonitrile (6136-68-1) + Glyoxilic acid (298-12-4) → 3-(6-oxo-1,6-dihydropyridazin-3-yl)-benzonitrile (52240-08-1)

Guidance literature:

3-acethylbenzonitrile; Glyoxilic acid; In acetic acid; acetone; at 95 ℃; for 18h;

With hydrazine hydrate; In water; acetic acid; at 30 - 95 ℃; for 4h;

Reference yield:

3-(6-chloropyridazin-3-yl)benzonitrile (99708-49-3) → 3-(6-oxo-1,6-dihydropyridazin-3-yl)-benzonitrile (52240-08-1)

Guidance literature:

With acetic acid; at 80 ℃; for 24h;

Reference yield:

→ 3-(6-oxo-1,6-dihydropyridazin-3-yl)-benzonitrile (52240-08-1)

Guidance literature:

Pyridazinon 14, Bromoxidation;

DOI:10.1021/jm00249a004

upstream raw materials:

3-acethylbenzonitrile

Glyoxilic acid

3-(6-chloropyridazin-3-yl)benzonitrile

Downstream raw materials:

3-[1-(4-bromothiophen-2-ylmethyl)-6-oxo-1,6-dihydropyridazin-3-yl]benzonitrile

3-{1-[6-(5-bromopyrimidin-2-yl)pyridin-2-ylmethyl]-6-oxo-1,6-dihydropyridazin-3-yl}benzonitrile

3-(6-oxo-1-{3-[5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-pyrimidin-2-yl]-benzyl}-1,6-dihydropyridazin-3-yl)-benzonitrile

3-{1-[3-(5-hydroxy-pyrimidin-2-yl)-benzyl]-6-oxo-1,6-dihydro-pyridazin-3-yl}-benzonitrile