tert-butyl azetidin-3-ylmethyl(methyl)carbamate

Base Information

• Chemical Name: tert-butyl azetidin-3-ylmethyl(methyl)carbamate
• CAS No.: 1053655-53-0
• Molecular Formula: C10H20N2O2
• Molecular Weight: 200.278
• Hs Code.: 2933990090
• Mol file: 1053655-53-0.mol

Synonyms:3-(N-Boc-Methylaminomethy...;

Chemical Property of tert-butyl azetidin-3-ylmethyl(methyl)carbamate

Chemical Property:

• Boiling Point: 267℃
• PKA: 10.86±0.40(Predicted)
• Flash Point: 116℃
• PSA: 50.36000
• Density: 1.012
• LogP: 0.85680
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99% ^*data from raw suppliers

tert-ButylAzetidin-3-ylmethyl(methyl)carbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl azetidin-3-ylmethyl(methyl)carbamate

There total 2 articles about tert-butyl azetidin-3-ylmethyl(methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H30N2O2 (1064048-70-9) → tert-butyl azetidin-3-yI(methyl)carbamate (1053655-53-0)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; at 20 ℃;

Reference yield:

[[1-(diphenylmethyl)-3-azetidinyl]methyl]-carbamic acid 1,1-dimethylethyl ester (91189-19-4) → tert-butyl azetidin-3-yI(methyl)carbamate (1053655-53-0)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; water; ethyl acetate; for 18h; Inert atmosphere;

Reference yield:

formic acid (64-18-6) + tert-butyl azetidin-3-yI(methyl)carbamate (1053655-53-0) + (R)-5-[2-(2-bromo-ethyl)-4-cyano-phenyl]-7-methyl-3-oxo-8-(3-trifluoromethyl-phenyl)-2,3,5,8-tetrahydro-[1,2,4] triazolo[4,3-a]pyrimidine-6-carboxylic acid methyl ester (1613621-76-3) → CH2O2*C29H30F3N7O3

Guidance literature:

tert-butyl azetidin-3-yI(methyl)carbamate; (R)-5-[2-(2-bromo-ethyl)-4-cyano-phenyl]-7-methyl-3-oxo-8-(3-trifluoromethyl-phenyl)-2,3,5,8-tetrahydro-[1,2,4] triazolo[4,3-a]pyrimidine-6-carboxylic acid methyl ester; With trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 3.5h;

formic acid; In water; acetonitrile; at 40 ℃;

upstream raw materials:

C₂₃H₃₀N₂O₂

[[1-(diphenylmethyl)-3-azetidinyl]methyl]-carbamic acid 1,1-dimethylethyl ester

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