N-Boc-4-MethylpiperidinecarbothioaMide

Base Information

Chemical Name:N-Boc-4-MethylpiperidinecarbothioaMide
CAS No.:951745-01-0
Molecular Formula:C12H22N2O2S
Molecular Weight:258.385
Hs Code.:
Mol file:951745-01-0.mol

Synonyms:MD-0790

Suppliers and Price of N-Boc-4-MethylpiperidinecarbothioaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
N-Boc-4-methylpiperidinecarbothioamide 95%
5g
$ 1876.00

Total 9 raw suppliers

Chemical Property of N-Boc-4-MethylpiperidinecarbothioaMide

Chemical Property:

PSA：87.65000
LogP:2.94790

Purity/Quality:

98%min ^*data from raw suppliers

N-Boc-4-methylpiperidinecarbothioamide 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Boc-4-MethylpiperidinecarbothioaMide

There total 3 articles about N-Boc-4-MethylpiperidinecarbothioaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 343788-67-0
4-carbamoyl-4-methylpiperidine-1-carboxylic acid tert-butyl ester

: 951745-01-0
4-methyl-4-thiocarbamoylpiperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: With Lawessons reagent; In 1,4-dioxane; at 20 ℃; for 15h;

Reference yield:

: 91419-52-2
1-tert-butoxycarbonyl-4-cyanopiperidine

: 951745-01-0
4-methyl-4-thiocarbamoylpiperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C

1.2: 2 h / 0 °C

2.1: sodium hydroxide; dihydrogen peroxide / methanol; dimethyl sulfoxide; water / 3 h / 50 °C

3.1: Lawessons reagent / tetrahydrofuran / 3 h / 50 °C

With Lawessons reagent; dihydrogen peroxide; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; water; dimethyl sulfoxide;

Reference yield:

: 530115-96-9
4-cyano-4-methylpiperidine-1-carboxylic acid tert-butyl ester

: 951745-01-0
4-methyl-4-thiocarbamoylpiperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; dihydrogen peroxide / methanol; dimethyl sulfoxide; water / 3 h / 50 °C

2: Lawessons reagent / tetrahydrofuran / 3 h / 50 °C

With Lawessons reagent; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; water; dimethyl sulfoxide;