2-(CYCLOHEXYLOXY)ETHANOL 99

Base Information

• Chemical Name: 2-(CYCLOHEXYLOXY)ETHANOL 99
• CAS No.: 1817-88-5
• Molecular Formula: C8H16 O2
• Molecular Weight: 144.214
• Hs Code.: 2909499000
• Mol file: 1817-88-5.mol

Synonyms:(2-Hydroxyethoxy)cyclohexane;2-Cyclohexyloxyethanol; Cyclohexyl cellosolve; Cyclohexyloxyethyl alcohol; NSC13548

Chemical Property of 2-(CYCLOHEXYLOXY)ETHANOL 99

Chemical Property:

• Vapor Pressure: 0.055mmHg at 25°C
• Refractive Index: n20/D 1.4630(lit.)
• Boiling Point: 206.7°Cat760mmHg
• Flash Point: 95°C
• PSA: 29.46000
• Density: 0.98g/cm³
• LogP: 1.32800

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-(Cyclohexyloxy)ethanol ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 2-(CYCLOHEXYLOXY)ETHANOL 99

There total 13 articles about 2-(CYCLOHEXYLOXY)ETHANOL 99 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.2%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + ethylene glycol (107-21-1) → 2-Cyclohexyloxyethanol (1817-88-5)

Guidance literature:

With chitosan immobilized with 3-(3-vinylimidazolyl)propane-1-sulfonate and 12-phosphotungstic acid; In cyclohexane; at 80 ℃; for 2h; Reflux; Dean-Stark;

DOI:10.1039/c6ra02169g

Reference yield: 87.0%

1,3-dioxolane-2-spirocyclohexane (177-10-6) → 2-Cyclohexyloxyethanol (1817-88-5)

Guidance literature:

With boron trifluoride diethyl etherate; sodium cyanoborohydride; In tetrahydrofuran; for 6h; Ambient temperature;

DOI:10.1016/0040-4020(95)00055-D

Reference yield:

2-(cyclohexyloxy)acetic acid (71995-54-5) → 2-Cyclohexyloxyethanol (1817-88-5)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

upstream raw materials:

1,3-dioxolane-2-spirocyclohexane

diethyl ether

2-(cyclohexyloxy)acetic acid

ethyl bromoacetate

Downstream raw materials:

Ethylenglycol-undecylether-cyclohexylether

cyclohexyl ethyl ether

2-(Cyclohexyloxy)-ethyl-trimethylsilylether

methanesulfonic acid 2-cyclohexyloxy-ethyl ester

Refernces

• 1、 Zhang, Wei-Hong,Liu, Shan-Shan,Liu, Ping,Xu, Jie,Xue, Bing,Wei, Xian-Yong,Li, Yong-Xin. "Chitosan grafted with a heteropolyanion-based ionic liquid as an effective and reusable catalyst for acetalization". . p. 41404 - 41409. Retrieved 2016/05/19.
• 2、 Purushothama Chary,Santosh Laxmi,Iyengar. "Reductive cleavage of acetals/ketals with ZrCl4/NaBH4". . p. 1257 - 1261. Retrieved 2007/10/03.