2'-Aminoacetophenonephenylhydrazone

Base Information

• Chemical Name: 2'-Aminoacetophenonephenylhydrazone
• CAS No.: 40754-13-0
• Molecular Formula: C14H15N3
• Molecular Weight: 225.293
• Hs Code.: 2928000090
• European Community (EC) Number: 631-019-8
• Nikkaji Number: J1.868.095E
• Mol file: 40754-13-0.mol

Synonyms:2'-Aminoacetophenone phenylhydrazone;(E)-2-(1-(2-Phenylhydrazono)ethyl)aniline;2'-AMINOACETOPHENONEPHENYLHYDRAZONE

Chemical Property of 2'-Aminoacetophenonephenylhydrazone

Chemical Property:

• Melting Point: 104-108 °C(lit.)
• Boiling Point: 384.868oC at 760 mmHg
• Flash Point: 186.562oC
• PSA: 50.41000
• Density: 1.092g/cm3
• LogP: 3.75910
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 225.126597491
• Heavy Atom Count: 17
• Complexity: 256

Purity/Quality:

99% ^*data from raw suppliers

2′-Aminoacetophenone phenylhydrazone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

Useful:

• Canonical SMILES: CC(=NNC1=CC=CC=C1)C2=CC=CC=C2N
• Isomeric SMILES: C/C(=N/NC1=CC=CC=C1)/C2=CC=CC=C2N

Technology Process of 2'-Aminoacetophenonephenylhydrazone

There total 2 articles about 2'-Aminoacetophenonephenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

→ 2-(1-(2-phenylhydrazineylidene)ethyl)aniline (40754-13-0)

Guidance literature:

Reference yield: 83.0%

2-aminoacetophenone (551-93-9) + phenylhydrazine (100-63-0) → 2-(1-(2-phenylhydrazineylidene)ethyl)aniline (40754-13-0)

Guidance literature:

With acetic acid; In ethanol; for 5h; Heating;

Reference yield: 90.0%

2-(1-(2-phenylhydrazineylidene)ethyl)aniline (40754-13-0) → 2-(2-aminophenyl)-1H-indole (32566-01-1)

Guidance literature:

With methanesulfonic acid; phosphorus pentoxide; at 80 ℃; for 0.5h;

DOI:10.1021/jo00101a043

upstream raw materials:

2-aminoacetophenone

phenylhydrazine

Downstream raw materials:

2-(2-aminophenyl)-1H-indole

5,6-dihydroindolo<1,2-c>quinazoline

2-Indolo[1,2-c]quinazolin-12-yl-N-(2-phenylselanyl-ethyl)-acetamide

2-(5,6-Dihydro-indolo[1,2-c]quinazolin-12-yl)-N-(2-phenylselanyl-ethyl)-acetamide

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