2-(3-(difluoroMethoxy)phenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3-(difluoroMethoxy)phenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane
CAS No.:1035690-56-2
Molecular Formula:C13H17BF2O3
Molecular Weight:270.084
Hs Code.:
Mol file:1035690-56-2.mol

Synonyms:2-(3-(difluoroMethoxy)phenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane;1,3,2-Dioxaborolane, 2-[3-(difluoromethoxy)phenyl]-4,4,5,5-tetramethyl-

Suppliers and Price of 2-(3-(difluoroMethoxy)phenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Ambeed
2-(3-(Difluoromethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 97%
1g
$ 212.00

Ambeed
2-(3-(Difluoromethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 97%
250mg
$ 77.00

Ambeed
2-(3-(Difluoromethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 97%
100mg
$ 49.00

AK Scientific
2-[3-(difluoromethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
1g
$ 512.00

Total 7 raw suppliers

Chemical Property of 2-(3-(difluoroMethoxy)phenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

Chemical Property:

Boiling Point:326.1±37.0 °C(Predicted)
PSA：27.69000
Density:1.13±0.1 g/cm3(Predicted)
LogP:2.58720

Purity/Quality:

97% ^*data from raw suppliers

2-(3-(Difluoromethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(3-(difluoroMethoxy)phenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane

There total 3 articles about 2-(3-(difluoroMethoxy)phenyl)-4,4,5,5-tetraMethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 73183-34-3
bis(pinacol)diborane

: 262587-05-3
(3-bromophenyl)difluoromethyl ether

: 1035690-56-2
2-(3-(difluoromethoxy)phenyl )-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With 10H-phenothiazine; caesium carbonate; In acetonitrile; for 48h; Irradiation; Sealed tube; Inert atmosphere;
DOI:10.1021/jacs.9b12519

Reference yield:

: 591-20-8
3-Bromophenol

: 1035690-56-2
2-(3-(difluoromethoxy)phenyl )-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 100 °C

2: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 21 h / 100 °C / Inert atmosphere

With potassium acetate; caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 1035690-56-2
2-(3-(difluoromethoxy)phenyl )-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 100 ℃; for 4h;