N-Boc-2-trimethylsilyl-1H-pyrrole

Base Information

Chemical Name:N-Boc-2-trimethylsilyl-1H-pyrrole
CAS No.:75400-57-6
Molecular Formula:C₁₂H₂₁NO₂Si
Molecular Weight:239.39
Hs Code.:
European Community (EC) Number:804-394-2
Nikkaji Number:J2.586.373I
Mol file:75400-57-6.mol

Synonyms:75400-57-6;tert-Butyl 2-(trimethylsilyl)-1H-pyrrole-1-carboxylate;N-Boc-2-trimethylsilyl-1H-pyrrole;N-Boc-2-trimethylsilyl-1H-pyrrole, 95%

Suppliers and Price of N-Boc-2-trimethylsilyl-1H-pyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-Boc-2-trimethylsilyl-1H-pyrrole 95%
1g
$ 93.50

Total 5 raw suppliers

Chemical Property of N-Boc-2-trimethylsilyl-1H-pyrrole

Chemical Property:

Melting Point:30-35°C
Flash Point:108℃
PSA：31.23000
LogP:2.81650
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:239.134155447
Heavy Atom Count:16
Complexity:265

Purity/Quality:

98%min ^*data from raw suppliers

N-Boc-2-trimethylsilyl-1H-pyrrole 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)N1C=CC=C1[Si](C)(C)C

Technology Process of N-Boc-2-trimethylsilyl-1H-pyrrole

There total 5 articles about N-Boc-2-trimethylsilyl-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 75-77-4
chloro-trimethyl-silane

: 5176-27-2
N-tert-butyloxycarbonyl-pyrrole

: 75400-57-6
N-(tert-butoxycarbonyl)-2-(trimethylsilyl)pyrrole

Guidance literature:: N-tert-butyloxycarbonyl-pyrrole; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 6h;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 10h; Further stages.;
DOI:10.1002/anie.200705005

Reference yield: 85.0%

: 75-77-4
chloro-trimethyl-silane

: 117657-37-1
2-bromo-pyrrole-1-carboxylic acid tert-butyl ester

: 75400-57-6
N-(tert-butoxycarbonyl)-2-(trimethylsilyl)pyrrole

Guidance literature:: 2-bromo-pyrrole-1-carboxylic acid tert-butyl ester; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -30 ℃; for 1h; Inert atmosphere;
DOI:10.15227/orgsyn.070.0151