tert-butyl Methyl(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbaMate

Base Information

Chemical Name:tert-butyl Methyl(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbaMate
CAS No.:817618-57-8
Molecular Formula:C18H28BNO4
Molecular Weight:333.236
Hs Code.:2934999090
Mol file:817618-57-8.mol

Synonyms:Carbamic acid, methyl[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-, 1,1-dimethylethyl ester (9CI);N-Methyl-N-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]carbamic acid tert-butyl ester;tert-Butyl N-Methyl[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]carbamate;

Suppliers and Price of tert-butyl Methyl(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbaMate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butylmethyl(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate 95+%
1g
$ 772.00

Chemenu
tert-Butylmethyl(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate 95%
1g
$ 615.00

American Custom Chemicals Corporation
TERT-BUTYL-METHYL(3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYL)CARBAMATE 95.00%
1G
$ 1575.00

American Custom Chemicals Corporation
TERT-BUTYL-METHYL(3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYL)CARBAMATE 95.00%
5MG
$ 496.54

Alichem
tert-Butylmethyl(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate
1g
$ 646.84

Total 5 raw suppliers

Chemical Property of tert-butyl Methyl(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbaMate

Chemical Property:

PSA：48.00000
LogP:3.35710
Storage Temp.:2-8°C

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

tert-Butylmethyl(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-butyl Methyl(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbaMate

There total 5 articles about tert-butyl Methyl(3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 57598-34-2
3-Bromo-N-tert-butoxycarbonyl-N-methylaniline

: 73183-34-3
bis(pinacol)diborane

: 817618-57-8
tert-butyl methyl-[3-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]carbamate

Guidance literature:: With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In N,N-dimethyl-formamide; at 80 ℃; for 6.25h;

Reference yield: 91.0%

: 28131-24-0
tert-butyl N-methyl-N-(phenyl)carbamate

: 73183-34-3
bis(pinacol)diborane

: 817618-57-8
tert-butyl methyl-[3-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]carbamate

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; C₁₉H₁₃N₃O; potassium tert-butylate; In tetrahydrofuran; at 80 ℃; for 12h; Reagent/catalyst; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1002/anie.201809929

Reference yield: 88.0%

: 330793-09-4
tert-butyl N-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl]carbamate

: 74-88-4
methyl iodide

: 817618-57-8
tert-butyl methyl-[3-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]carbamate

Guidance literature:: tert-butyl N-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl]carbamate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/acs.jmedchem.7b01356