4-cyclopropyl-1-fluoro-2-nitrobenzene

Base Information

• Chemical Name: 4-cyclopropyl-1-fluoro-2-nitrobenzene
• CAS No.: 769159-85-5
• Molecular Formula: C9H8FNO2
• Molecular Weight: 181.166
• Hs Code.: 2904990090
• Mol file: 769159-85-5.mol

Synonyms:4-fluoro-3-nitrocyclopropylbenzene;4-fluoro-3-nitro-1-cyclopropylbenzene;QC-2776;RW3632;

Chemical Property of 4-cyclopropyl-1-fluoro-2-nitrobenzene

Chemical Property:

• PSA: 45.82000
• LogP: 3.13450

Purity/Quality:

97% ^*data from raw suppliers

4-Cyclopropyl-1-fluoro-2-nitrobenzene 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-cyclopropyl-1-fluoro-2-nitrobenzene

There total 2 articles about 4-cyclopropyl-1-fluoro-2-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4-Bromo-1-fluoro-2-nitrobenzene (364-73-8) + cyclopropylboronic acid (411235-57-9) → 4-cyclopropyl-1-fluoro-2-nitrobenzene (769159-85-5)

Guidance literature:

With potassium phosphate tribasic heptahydrate; C₄₅H₅₃ClFeNO₂PPd; In water; toluene; at 100 ℃; for 10h; Inert atmosphere;

DOI:10.1016/j.tet.2011.11.024

Reference yield:

1-fluoro-4-iodo-2-nitro-benzene (364-75-0) + tri(cyclopropyl)indium (23719-81-5) → 4-cyclopropyl-1-fluoro-2-nitrobenzene (769159-85-5)

Guidance literature:

Reference yield:

4-cyclopropyl-1-fluoro-2-nitrobenzene (769159-85-5) → 5-cyclopropyl-2-fluoroaniline (1374298-69-7)

Guidance literature:

4-cyclopropyl-1-fluoro-2-nitrobenzene; With iron; acetic acid; at 22 - 26 ℃; for 2h;

With sodium hydrogencarbonate; In water;

upstream raw materials:

1-fluoro-4-iodo-2-nitro-benzene

tri(cyclopropyl)indium

4-Bromo-1-fluoro-2-nitrobenzene

cyclopropylboronic acid

Downstream raw materials:

4-cyclopropyl-2-nitro-N-(3-(3-pyridyl)phenyl)aniline

5-cyclopropyl-2-fluoroaniline

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