Tricyclopropylindium

Base Information Edit

Chemical Name:Tricyclopropylindium
CAS No.:23719-81-5
Molecular Formula:C9H15In
Molecular Weight:238.038
Hs Code.:
DSSTox Substance ID:DTXSID401315252
Mol file:23719-81-5.mol

Synonyms:Tricyclopropylindium;23719-81-5;DTXSID401315252

Suppliers and Price of Tricyclopropylindium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tricyclopropylindium Edit

Chemical Property:

PSA：0.00000
LogP:3.35400
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:238.0212543
Heavy Atom Count:10
Complexity:114

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC1[In](C2CC2)C3CC3

Technology Process of Tricyclopropylindium

There total 3 articles about Tricyclopropylindium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 7440-74-6
indium

: 13955-96-9
Dicyclopropyl-quecksilber

: 23719-81-5
tri(cyclopropyl)indium

Guidance literature:: In neat (no solvent); The reactants in sealed tube were heated in an oil bath to 70°C for 1 week;; distilled at 80°C and 10E-6 torr;;
DOI:10.1021/om00064a001

Reference yield:

: indium(III) chloride

: 4333-56-6,130561-87-4
cyclopropyl bromide

: 23719-81-5
tri(cyclopropyl)indium

Guidance literature:: cyclopropyl bromide; With tert.-butyl lithium; at -78 ℃; Inert atmosphere;

indium(III) chloride; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.6b02058

Reference yield:

: 10025-82-8
indium(III) chloride

: 3002-94-6
cyclopropyllithium

: 23719-81-5
tri(cyclopropyl)indium

Guidance literature:: In not given; under Ar; cyclo-C3H5Li (3 equiv.) in THF or hexane or Et2O added slowly (15-30 min) to cooled (-78°C) soln. of InCl3 in THF; stirred for 30 min; warmed to room temp.; according to H. C. Clark, A. L. Pickard, J. Organomet. Chem. 8 (1967) 427;
DOI:10.1021/ja004195m