Technology Process of 7-methoxy-6-methyl-2,3-dihydro-1H-indene-4-carbaldehyde
There total 1 articles about 7-methoxy-6-methyl-2,3-dihydro-1H-indene-4-carbaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 0 - 30 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium tetrahydroborate / methanol / 2 h / 10 - 20 °C
1.2: pH 6
1.3: 2 h / 10 - 25 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 2.5 - 3 h / 40 - 45 °C
2.2: 1 h / 15 - 85 °C
2.3: 11 - 12 h / Heating / reflux
3.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 25 - 30 °C
4.1: hydrazine / 3 h / 60 - 65 °C
With
sodium tetrahydroborate; potassium carbonate; caesium carbonate; hydrazine;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate / methanol / 2 h / 10 - 20 °C
1.2: pH 6
1.3: 2 h / 10 - 25 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 2.5 - 3 h / 40 - 45 °C
2.2: 1 h / 15 - 85 °C
2.3: 11 - 12 h / Heating / reflux
3.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 25 - 30 °C
4.1: methanol; sodium hydroxide; water / tetrahydrofuran / 1.5 - 2 h / 20 - 30 °C
5.1: boron tribromide / dichloromethane / 2 - 3 h / 0 - 30 °C
5.2: 1 h
With
methanol; sodium hydroxide; sodium tetrahydroborate; water; boron tribromide; potassium carbonate; caesium carbonate;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
