4-tert-Butyl-5-chloro-2-hydroxybenzaldehyde

Base Information

• Chemical Name: 4-tert-Butyl-5-chloro-2-hydroxybenzaldehyde
• CAS No.: 914225-72-2
• Molecular Formula: C₁₁H₁₃ClO₂
• Molecular Weight: 212.676
• Hs Code.: 2913000090
• Mol file: 914225-72-2.mol

Synonyms:4-TERT-BUTYL-5-CHLORO-2-HYDROXYBENZALDE; Benzaldehyde, 5-chloro-4-(1,1-dimethylethyl)-2-hydroxy-

Chemical Property of 4-tert-Butyl-5-chloro-2-hydroxybenzaldehyde

Chemical Property:

• PSA: 37.30000
• LogP: 3.15560

Purity/Quality:

97% ^*data from raw suppliers

4-tert-Butyl-5-chloro-2-hydroxybenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-tert-Butyl-5-chloro-2-hydroxybenzaldehyde

There total 3 articles about 4-tert-Butyl-5-chloro-2-hydroxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hexamethylenetetramine (100-97-0) + 3-(tert-butyl)-4-chlorophenol (90875-84-6) → 4-tert-butyl-5-chloro-2-hydroxybenzaldehyde (914225-72-2)

Guidance literature:

With methanesulfonic acid; at 0 - 100 ℃;

Reference yield:

methanesulfonic acid (75-75-2,98527-29-8) + 3-(tert-butyl)-4-chlorophenol (90875-84-6) → 4-tert-butyl-5-chloro-2-hydroxybenzaldehyde (914225-72-2)

Guidance literature:

With hexamethylenetetramine; at 0 - 100 ℃;

Reference yield:

3-tert-butylphenyol (585-34-2) → 4-tert-butyl-5-chloro-2-hydroxybenzaldehyde (914225-72-2)

Guidance literature:

Multi-step reaction with 2 steps

1: iron(III) chloride; sulfuryl dichloride / dichloromethane / 60 °C

2: methanesulfonic acid / 0 - 100 °C

With iron(III) chloride; sulfuryl dichloride; methanesulfonic acid; In dichloromethane;

upstream raw materials:

3-tert-butylphenyol

hexamethylenetetramine

3-(tert-butyl)-4-chlorophenol

methanesulfonic acid

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