1-Nitroso-2,2,6,6-tetramethylpiperidine

Base Information

Chemical Name:1-Nitroso-2,2,6,6-tetramethylpiperidine
CAS No.:6130-93-4
Molecular Formula:C9H18 N2 O
Molecular Weight:170.255
Hs Code.:2933399090
DSSTox Substance ID:DTXSID50879627
Nikkaji Number:J2.240C
Wikidata:Q82861733
ChEMBL ID:CHEMBL165516
Mol file:6130-93-4.mol

Synonyms:2,2',6,6'-tetramethyl-N-nitrosopiperidine

Suppliers and Price of 1-Nitroso-2,2,6,6-tetramethylpiperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 1-Nitroso-2,2,6,6-tetramethylpiperidine

Chemical Property:

Vapor Pressure:0.0434mmHg at 25°C
Refractive Index:1.4790 (estimate)
Boiling Point:246.1°C at 760 mmHg
Flash Point:102.6°C
PSA：98.13000
Density:1g/cm³
LogP:2.95150
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:170.141913202
Heavy Atom Count:12
Complexity:171

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Chemical Classes:Nitrogen Compounds -> Nitrosamines
Canonical SMILES:CC1(CCCC(N1N=O)(C)C)C
Uses 2,?2'',?6,?6''-?Tetramethyl-?N-?nitrosopiperidine is a non-carcinogenic derivative of N-?nitrosopiperidine.

Technology Process of 1-Nitroso-2,2,6,6-tetramethylpiperidine

There total 5 articles about 1-Nitroso-2,2,6,6-tetramethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1393481-89-4
1-(phenylethynyl)-2-(vinyloxy)-benzene

: 6130-93-4
2,2,6,6-tetramethyl-1-nitrosopiperidine

: 3-benzoylbenzofuran-2-carbaldehyde

Guidance literature:: With tert.-butylnitrite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In N,N-dimethyl-formamide; at 40 ℃; for 8h; under 760.051 Torr; Schlenk technique;
DOI:10.1002/anie.201408978

Reference yield: 68.0%

: 768-66-1
2,2,6,6-tetramethyl-piperidine

: 6130-93-4
2,2,6,6-tetramethyl-1-nitrosopiperidine

: 24192-33-4
N-fluoro-2,2,6,6-tetramethylpiperidine

Guidance literature:: With trifluoroamine oxide; at 0 ℃; for 12h;
DOI:10.1021/ja00162a045

Reference yield: 50.0%

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 75-52-5
nitromethane

: 4424-17-3
2-aminobenzanilide

: 16347-60-7
3-phenyl-4(3H)-quinazolinone

: 6130-93-4
2,2,6,6-tetramethyl-1-nitrosopiperidine

: 19263-30-0
3-phenyl-1,2,3-benzotriazin-4(3H)-one

Guidance literature:: With tert.-butylhydroperoxide; caesium carbonate; acetic acid; potassium iodide; In water; at 120 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1002/adsc.201500619