Diallyl succinate

Base Information

• Chemical Name: Diallyl succinate
• CAS No.: 925-16-6
• Deprecated CAS: 150154-40-8
• Molecular Formula: C10H14 O4
• Molecular Weight: 198.219
• Hs Code.: 2917190090
• European Community (EC) Number: 213-115-8
• NSC Number: 20965
• UNII: AMT9NLX4PW
• DSSTox Substance ID: DTXSID1061287
• Nikkaji Number: J147.943A
• Wikidata: Q81989400
• Mol file: 925-16-6.mol

Synonyms:Diallyl succinate;925-16-6;bis(prop-2-enyl) butanedioate;Butanedioic acid, di-2-propenyl ester;Succinic acid, diallyl ester;JF 2777;JF 3958;AMT9NLX4PW;Butanedioic acid, 1,4-di-2-propen-1-yl ester;Butanoic acid, di-2-propenyl ester;EINECS 213-115-8;NSC 20965;NSC-20965;AI3-05546;Diallylsuccinate;UNII-AMT9NLX4PW;Diallyl succinate, 97%;SCHEMBL56403;DTXSID1061287;NSC20965;AKOS015915997;1,4-bis(prop-2-en-1-yl) butanedioate;butanedioic acid bis(prop-2-enyl) ester;butanedioic acid bis-(prop-2-enyl) ester;FT-0624604;A845836

Chemical Property of Diallyl succinate

Chemical Property:

• Vapor Pressure: 0.0108mmHg at 25°C
• Refractive Index: n20/D 1.454(lit.)
• Boiling Point: 262.6°Cat760mmHg
• Flash Point: 116.7°C
• PSA: 52.60000
• Density: 1.039g/cm³
• LogP: 1.22500
• Storage Temp.: Room Temperature
• Solubility.: Chloroform (Slightly), Methanol (Slightly)
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 9
• Exact Mass: 198.08920892
• Heavy Atom Count: 14
• Complexity: 196

Purity/Quality:

99% ^*data from raw suppliers

DiallylSuccinate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C=CCOC(=O)CCC(=O)OCC=C
• Uses: Diallyl Succinate is used in the synthesis of crosslinked polymers as well as for magnetic polyethylenamine complexes for use in enhancing gene transfection.

Technology Process of Diallyl succinate

There total 7 articles about Diallyl succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

succinic acid (110-15-6) + allyl alcohol (107-18-6) → diallyl succinate (925-16-6)

Guidance literature:

With 3,3′-(2,2-bis(hydroxymethyl)propane-1,3-diyl)bis(1-methyl-1H-imidazol-3-ium) hydrogen sulfate; for 3h; Dean-Stark; Reflux;

DOI:10.1016/j.molliq.2016.11.121

Reference yield: 99.0%

diallyl maleate (999-21-3) → diallyl succinate (925-16-6)

Guidance literature:

With 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; phenylsilane; water; In toluene; at 80 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.201912991

Reference yield: 88.0%

succinic acid (110-15-6) + allyl bromide (106-95-6) → diallyl succinate (925-16-6)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1002/ejoc.201301239

upstream raw materials:

succinic acid anhydride

allyl alcohol

succinic acid

3-chloroprop-1-ene

Downstream raw materials:

2,5-dioxo-cyclohexane-1,4-dicarboxylic acid diallyl ester

diallyl 2,5-dihydroxycyclohexa-1,4-diene-1,4-dicarboxylate

diallyl 2-benzoylsuccinate

2-chloro-3-(2-chlorophenyl)propyl 3-carballyloxypropionate