2-CarbaMoylfuran-4-boronic acid pinacol ester, 96%

Base Information

Chemical Name:2-CarbaMoylfuran-4-boronic acid pinacol ester, 96%
CAS No.:957345-98-1
Molecular Formula:C₁₁H₁₆BNO₄
Molecular Weight:237.063
Hs Code.:
Mol file:957345-98-1.mol

Synonyms:4-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)furan-2-carboxylic acid amide;4-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)furan-2-carboxamide;

Suppliers and Price of 2-CarbaMoylfuran-4-boronic acid pinacol ester, 96%

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Advanced Chemicals Intermediatesced Chemicals Intermediates
4-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-furan-2-carboxylicacidamide 95%+
1g
$ 862.75

Acints
4-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-furan-2-carboxylicacidamide 95%+
1g
$ 862.75

Total 2 raw suppliers

Chemical Property of 2-CarbaMoylfuran-4-boronic acid pinacol ester, 96%

Chemical Property:

Boiling Point:363.0±27.0 °C (760 mmHg)
PSA：74.69000
Density:1.16±0.1 g/cm3 (20 °C, 760 mmHg)
LogP:1.37800

Purity/Quality:

99% ^*data from raw suppliers

4-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-furan-2-carboxylicacidamide 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-CarbaMoylfuran-4-boronic acid pinacol ester, 96%

There total 5 articles about 2-CarbaMoylfuran-4-boronic acid pinacol ester, 96% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 957345-95-8
4-bromo-furan-2-carboxylic acid amide

: 73183-34-3
bis(pinacol)diborane

: 957345-98-1
4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-furan-2-carboxylic acid amide

Guidance literature:: With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 85 ℃; Inert atmosphere;

Reference yield:

: 1189-71-5
isocyanate de chlorosulfonyle

: 248924-59-6
3-furylboronic acid pinacol ester

: 957345-98-1
4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-furan-2-carboxylic acid amide

Guidance literature:: isocyanate de chlorosulfonyle; 3-furylboronic acid pinacol ester; In acetonitrile; at 20 ℃;

With water; In acetonitrile; Cooling with ice;

Reference yield:

: 2434-03-9
4,5-dibromo-2-furoic acid

: 957345-98-1
4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-furan-2-carboxylic acid amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium hydroxide; zinc / water / 20 °C / Cooling

1.2: -10 °C / pH 1

2.1: thionyl chloride / 1 h / Reflux

3.1: ammonia / dichloromethane; 1,4-dioxane / 1 h / 20 °C / Reflux

3.2: 2 h / 20 °C

4.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 85 °C / Inert atmosphere

With ammonium hydroxide; thionyl chloride; ammonia; potassium acetate; zinc; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; dichloromethane; water;