3-Bromo-4-iodophenol 97%

Base Information

Chemical Name:3-Bromo-4-iodophenol 97%
CAS No.:1037298-05-7
Molecular Formula:C6H4BrIO
Molecular Weight:298.906
Hs Code.:2908190090
Mol file:1037298-05-7.mol

Synonyms:3-bromo-4-imino-3-cyano-1,2,3,4-tetrahydrospiro(naphthalene-2,1'-cyclohexane);3',4'-Dihydro-3'-bromo-4'-iminospiro(cyclohexane-1,2'-(1'H)naphthalene)-3'-carbonitrile;Spiro(cyclohexane-1,2'(1'H)-naphthalene)-3'-carbonitrile,3',4'-dihydro-3'-bromo-4'-imino;3-bromo-4-iodophenol;

Suppliers and Price of 3-Bromo-4-iodophenol 97%

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Bromo-4-iodophenol
10mg
$ 45.00

SynQuest Laboratories
3-Bromo-4-iodophenol 97%
250 mg
$ 192.00

SynQuest Laboratories
3-Bromo-4-iodophenol 97%
1 g
$ 448.00

Chemcia Scientific
3-Bromo-4-iodo-phenol 95%
2.5 G
$ 725.00

Apolloscientific
3-Bromo-4-iodophenol 97%
1g
$ 378.00

Apolloscientific
3-Bromo-4-iodophenol 97%
250mg
$ 163.00

Ambeed
3-Bromo-4-iodophenol 98%
5g
$ 61.00

Ambeed
3-Bromo-4-iodophenol 98%
1g
$ 19.00

Ambeed
3-Bromo-4-iodophenol 98%
250mg
$ 9.00

Ambeed
3-Bromo-4-iodophenol 98%
100mg
$ 6.00

Total 12 raw suppliers

Chemical Property of 3-Bromo-4-iodophenol 97%

Chemical Property:

PSA：20.23000
LogP:2.75930

Purity/Quality:

97% ^*data from raw suppliers

3-Bromo-4-iodophenol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Bromo-4-iodophenol 97%

There total 5 articles about 3-Bromo-4-iodophenol 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428963-74-9
3-bromo-4-iodophenyl methanesulfonate

: 1037298-05-7
3-bromo-4-iodophenol

Guidance literature:: With potassium hydroxide; In methanol; dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol400597f

Reference yield:

: 20455-07-6
p-nitrophenyl methanesulfonate

: 1037298-05-7
3-bromo-4-iodophenol

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; hydrogen / ethyl acetate; ethanol / 3 h / 20 °C / 51683.5 Torr

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

3.1: sulfuric acid / water; acetonitrile / 0.17 h / 0 °C

3.2: 1.5 h / 0 - 5 °C

3.3: 0.25 h / 0 °C

4.1: potassium hydroxide / methanol; dichloromethane / 1 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; sulfuric acid; palladium 10% on activated carbon; hydrogen; potassium hydroxide; In methanol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol400597f

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1037298-05-7
3-bromo-4-iodophenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 0.75 h / 0 - 20 °C

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate; ethanol / 3 h / 20 °C / 51683.5 Torr

3.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

4.1: sulfuric acid / water; acetonitrile / 0.17 h / 0 °C

4.2: 1.5 h / 0 - 5 °C

4.3: 0.25 h / 0 °C

5.1: potassium hydroxide / methanol; dichloromethane / 1 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; sulfuric acid; palladium 10% on activated carbon; hydrogen; triethylamine; potassium hydroxide; In methanol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol400597f