2,5-dioxopyrrolidin-1-yl 6-(2-(propan-2-ylidene)hydrazinyl)nicotinate (S-SANH)

Base Information

• Chemical Name: 2,5-dioxopyrrolidin-1-yl 6-(2-(propan-2-ylidene)hydrazinyl)nicotinate (S-SANH)
• CAS No.: 362522-50-7
• Molecular Formula: C13H14N4O4
• Molecular Weight: 322.31982
• Mol file: 362522-50-7.mol

Synonyms:2,5-dioxopyrrolidin-1-yl 6-(2-(propan-2-ylidene)hydrazinyl)nicotinate (S-SANH);2,5-dioxopyrrolidin-1-yl 6-(2-(propan-2-ylidene)hydrazinyl)nicotinate;S-SANH;succiniMidyl 6-hydrazinonicotinate acetone hydrazone

Chemical Property of 2,5-dioxopyrrolidin-1-yl 6-(2-(propan-2-ylidene)hydrazinyl)nicotinate (S-SANH)

Chemical Property:

• PSA: 100.96000
• LogP: 1.12100
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2,5-Dioxopyrrolidin-1-yl6-(2-(propan-2-ylidene)hydrazinyl)nicotinate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5-dioxopyrrolidin-1-yl 6-(2-(propan-2-ylidene)hydrazinyl)nicotinate (S-SANH)

There total 1 articles about 2,5-dioxopyrrolidin-1-yl 6-(2-(propan-2-ylidene)hydrazinyl)nicotinate (S-SANH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + 6-hydrazinylnicotinic acid (133081-24-0) + acetone (67-64-1) → N-(2,5-dioxopyrrolidin-1-yl)-6-(2-(propan-2-ylidene)hydrazinyl)nicotinate (362522-50-7)

Guidance literature:

6-hydrazinylnicotinic acid; acetone; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Inert atmosphere;

1-hydroxy-pyrrolidine-2,5-dione; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; Inert atmosphere;

DOI:10.1021/ja304837f

Reference yield:

N-(2,5-dioxopyrrolidin-1-yl)-6-(2-(propan-2-ylidene)hydrazinyl)nicotinate (362522-50-7) + amino-Peg11 folate → folate-peg11-HyNic acetone hydrazone

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; for 1.5h;

Reference yield:

α-melanocyte stimulating hormone (581-05-5,75487-36-4) + N-(2,5-dioxopyrrolidin-1-yl)-6-(2-(propan-2-ylidene)hydrazinyl)nicotinate (362522-50-7) → C86H118N24O20S

Guidance literature:

In water; dimethyl sulfoxide; at 20 ℃; pH=8; HEPES buffer;

DOI:10.1021/ac9005233

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

6-hydrazinylnicotinic acid

acetone

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