7-beta-ribofuranosylhypoxanthine

Base Information

• Chemical Name: 7-beta-ribofuranosylhypoxanthine
• CAS No.: 10280-01-0
• Molecular Formula: C10H12 N4 O5
• Molecular Weight: 268.229
• Mol file: 10280-01-0.mol

Synonyms:Hypoxanthine,7-b-D-ribofuranosyl- (6CI,7CI,8CI);7-b-D-Ribofuranosylhypoxanthine

Chemical Property of 7-beta-ribofuranosylhypoxanthine

Chemical Property:

• Vapor Pressure: 1.52E-22mmHg at 25°C
• Boiling Point: 732.8°Cat760mmHg
• Flash Point: 397°C
• PSA: 133.49000
• Density: 2.08g/cm³
• LogP: -2.26890

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-beta-ribofuranosylhypoxanthine

There total 3 articles about 7-beta-ribofuranosylhypoxanthine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formic acid (64-18-6) + 5-amino-3-β-D-ribofuranosyl-3H-imidazole-4-carboxylic acid amide (7132-71-0) + acetic anhydride (108-24-7) → 7-β-D-ribofuranosyl-1,7-dihydro-purin-6-one (5627-15-6,5627-18-9,10280-01-0,10280-02-1,19895-30-8) + 1,7-dihydro-6H-purin-6-one (68-94-0)

Guidance literature:

und Erwaermen des Reaktionsprodukts mit wss.KHCO₃;

Reference yield:

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose (6974-32-9) + hypoxanthine (68-94-0) → Inosine (58-63-9) + 7-β-D-ribofuranosyl-1,7-dihydro-purin-6-one (10280-01-0)

Guidance literature:

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose; hypoxanthine; With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 130 ℃; for 0.0833333h; microwave irradiation;

With ammonia; In methanol; at 50 ℃; for 16h; Title compound not separated from byproducts;

DOI:10.1021/jo061885l

Reference yield:

→ 7-Ribofuranosyl-hypoxanthin (5627-15-6,5627-18-9,10280-01-0,10280-02-1,19895-30-8)

Guidance literature:

Triacetylribofuranosylchlorid, Hypoxanthin-silber-salz;

DOI:10.1016/S0040-4039(01)98881-1

upstream raw materials:

formic acid

5-amino-3-β-D-ribofuranosyl-3H-imidazole-4-carboxylic acid amide

acetic anhydride

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

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