3-CHLORO-5-FLUOROBENZOYL CHLORIDE

Base Information

• Chemical Name: 3-CHLORO-5-FLUOROBENZOYL CHLORIDE
• CAS No.: 886496-62-4
• Molecular Formula: C7H3Cl2FO
• Molecular Weight: 193.005
• Hs Code.: 2916399090
• Mol file: 886496-62-4.mol

Synonyms:3-CHLORO-5-FLUOROBENZOYL CHLORIDE

Chemical Property of 3-CHLORO-5-FLUOROBENZOYL CHLORIDE

Chemical Property:

• PSA: 17.07000
• LogP: 2.85810
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Chloro-5-fluorobenzoyl chloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-Chloro-5-fluoro-benzoyl chloride is a useful building block and has been used in the synthesis of 3,6-disubstituted-1,2,4,5-tetrazine derivatives as potential antitumor agents.

Technology Process of 3-CHLORO-5-FLUOROBENZOYL CHLORIDE

There total 2 articles about 3-CHLORO-5-FLUOROBENZOYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-chloro-5-fluoro-benzoic acid (25026-64-6) → 3-chloro-5-fluorobenzoyl chloride (886496-62-4)

Guidance literature:

With thionyl chloride; for 5h; Reflux;

Reference yield:

oxalyl dichloride (79-37-8) + 3-chloro-5-fluoro-benzoic acid (25026-64-6) → 3-chloro-5-fluorobenzoyl chloride (886496-62-4)

Guidance literature:

N,N-dimethyl-formamide; In dichloromethane;

Reference yield: 86.0%

3-chloro-5-fluorobenzoyl chloride (886496-62-4) + 1-(tert-butoxycarbonyl)-4-aminopiperidine (87120-72-7) → tert-butyl-4-(3-chloro-5-fluorobenzamido)piperidine-1-carboxylate

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1002/jhet.4368

upstream raw materials:

oxalyl dichloride

3-chloro-5-fluoro-benzoic acid

Downstream raw materials:

C₇H₆ClFN₂O

3-chloro-5-fluoro-N-methoxy-N-methylbenzamide

1-(3-chloro-5-fluorophenyl)propan-1-one

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