N-[2-[[[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl]amino]ethyl]carbamic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:N-[2-[[[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl]amino]ethyl]carbamic acid 1,1-dimethylethyl ester
CAS No.:1014613-14-9
Molecular Formula:C₁₉H₃₁BN₂O₆S
Molecular Weight:426.342
Hs Code.:
Mol file:1014613-14-9.mol

Synonyms:N-[2-[[[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl]amino]ethyl]carbamic acid 1,1-dimethylethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-[[[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl]amino]ethyl]carbamic acid 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-[2-[[[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl]amino]ethyl]carbamic acid 1,1-dimethylethyl ester

There total 4 articles about N-[2-[[[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl]amino]ethyl]carbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 928656-94-4
pentafluorophenyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonate

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1014613-14-9
1,1-dimethylethyl [2-({[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl}amino)ethyl]carbamate

Guidance literature:: With triethylamine; at 120 ℃; for 0.166667h; Microwave irradiation; Inert atmosphere;

Reference yield:

: 310480-85-4
tert-butyl (2-((4-Bromophenyl)sulfonamido)ethyl)carbamate

: 73183-34-3
bis(pinacol)diborane

: 1014613-14-9
1,1-dimethylethyl [2-({[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl}amino)ethyl]carbamate

Guidance literature:: With potassium acetate; palladium diacetate; In N,N-dimethyl-formamide; at 50 ℃; for 2h; Inert atmosphere;

Reference yield:

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1014613-14-9
1,1-dimethylethyl [2-({[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl}amino)ethyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 °C / Inert atmosphere

2: potassium acetate / palladium diacetate / N,N-dimethyl-formamide / 2 h / 50 °C / Inert atmosphere

With potassium acetate; triethylamine; palladium diacetate; In dichloromethane; N,N-dimethyl-formamide;