1,1-dimethylethyl {2-[({4-[2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridin-4-yl]phenyl}sulfonyl)amino]ethyl}carbamate

Base Information

Chemical Name:1,1-dimethylethyl {2-[({4-[2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridin-4-yl]phenyl}sulfonyl)amino]ethyl}carbamate
CAS No.:1187448-98-1
Molecular Formula:C₂₅H₃₄N₄O₄S
Molecular Weight:486.635
Hs Code.:

Synonyms:1,1-dimethylethyl {2-[({4-[2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridin-4-yl]phenyl}sulfonyl)amino]ethyl}carbamate

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Chemical Property of 1,1-dimethylethyl {2-[({4-[2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridin-4-yl]phenyl}sulfonyl)amino]ethyl}carbamate

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Technology Process of 1,1-dimethylethyl {2-[({4-[2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridin-4-yl]phenyl}sulfonyl)amino]ethyl}carbamate

There total 9 articles about 1,1-dimethylethyl {2-[({4-[2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridin-4-yl]phenyl}sulfonyl)amino]ethyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1014613-14-9
1,1-dimethylethyl [2-({[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]sulfonyl}amino)ethyl]carbamate

: 1187448-81-2
4-chloro-2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridine

: 1187448-98-1
1,1-dimethylethyl {2-[({4-[2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridin-4-yl]phenyl}sulfonyl)amino]ethyl}carbamate

Guidance literature:: With potassium phosphate; 2’-(dimethylamino)-2-biphenylyl-palladium(II)chloride dinorbornylphosphine complex; In 1,4-dioxane; water; at 140 ℃; for 0.5h; Microwave irradiation; Inert atmosphere;

Reference yield:

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1187448-98-1
1,1-dimethylethyl {2-[({4-[2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridin-4-yl]phenyl}sulfonyl)amino]ethyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 0.17 h / 120 °C / Microwave irradiation; Inert atmosphere

2: potassium phosphate / 2’-(dimethylamino)-2-biphenylyl-palladium(II)chloride dinorbornylphosphine complex / 1,4-dioxane; water / 0.5 h / 140 °C / Microwave irradiation; Inert atmosphere

With potassium phosphate; triethylamine; 2’-(dimethylamino)-2-biphenylyl-palladium(II)chloride dinorbornylphosphine complex; In 1,4-dioxane; water;

Reference yield:

: 630-18-2
tert-butyl isocyanide

: 1187448-98-1
1,1-dimethylethyl {2-[({4-[2-(1,1-dimethylethyl)-5-methyl-1H-pyrrolo[2,3-b]pyridin-4-yl]phenyl}sulfonyl)amino]ethyl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; ethylbenzene / 0 °C / Inert atmosphere

1.2: 0 - 5 °C / Inert atmosphere

1.3: 4 h / 60 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; ethyl acetate / 0 °C / Cooling with ice-NaCl

3.1: methanesulfonyl chloride / N,N-dimethyl-formamide / 1.25 h / 50 °C

4.1: potassium phosphate / 2’-(dimethylamino)-2-biphenylyl-palladium(II)chloride dinorbornylphosphine complex / 1,4-dioxane; water / 0.5 h / 140 °C / Microwave irradiation; Inert atmosphere

With potassium phosphate; methanesulfonyl chloride; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; 2’-(dimethylamino)-2-biphenylyl-palladium(II)chloride dinorbornylphosphine complex; In tetrahydrofuran; 1,4-dioxane; dichloromethane; ethylbenzene; water; ethyl acetate; N,N-dimethyl-formamide;