3aα,3bβ,6aβ,6bα-Tetrahydro-2,2,5,5-tetramethylcyclobuta[1,2-d:3,4-d']bis[1,3]dioxole

Base Information

• Chemical Name: 3aα,3bβ,6aβ,6bα-Tetrahydro-2,2,5,5-tetramethylcyclobuta[1,2-d:3,4-d']bis[1,3]dioxole
• CAS No.: 61845-71-4
• Molecular Weight: 200.23

Synonyms:3aα,3bβ,6aβ,6bα-Tetrahydro-2,2,5,5-tetramethylcyclobuta[1,2-d:3,4-d']bis[1,3]dioxole

Chemical Property of 3aα,3bβ,6aβ,6bα-Tetrahydro-2,2,5,5-tetramethylcyclobuta[1,2-d:3,4-d']bis[1,3]dioxole

Chemical Property:

• Boiling Point: 238.6±35.0 °C(Predicted)
• Density: 1.109±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 3aα,3bβ,6aβ,6bα-Tetrahydro-2,2,5,5-tetramethylcyclobuta[1,2-d:3,4-d']bis[1,3]dioxole

There total 4 articles about 3aα,3bβ,6aβ,6bα-Tetrahydro-2,2,5,5-tetramethylcyclobuta[1,2-d:3,4-d']bis[1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dimethyl-[1,3]dioxole (22945-10-4) + benzonitrile (100-47-0) → trans 1,2,3,4-bis(isopropylidenedioxy)-cyclobutane (61845-71-4,110549-41-2)

Guidance literature:

In cyclohexane; for 5h; Yield given; Irradiation;

DOI:10.1016/S0040-4020(01)96635-9

Reference yield:

2,2-dimethyl-[1,3]dioxole (22945-10-4) + methoxybenzene (100-66-3) → trans 1,2,3,4-bis(isopropylidenedioxy)-cyclobutane (61845-71-4,110549-41-2) + exo-6,7-isopropylidenedioxy-1-methoxytricyclo<3.3.0.02.8>-oct-3-en (108805-95-4,108866-86-0) + endo-6,7-isopropylidenedioxy-1-methoxytricyclo<3.3.0.02.8>-oct-3-en (108805-95-4,108866-86-0) + exo-7,8-isopropylidenedioxy-1-methoxybicyclo<4.2.0>octa-2,4-diene (108805-96-5,108866-87-1)

Guidance literature:

In 1,4-dioxane; Yield given. Further byproducts given. Yields of byproduct given; Irradiation;

Reference yield:

2,2-dimethyl-[1,3]dioxole (22945-10-4) + methoxybenzene (100-66-3) → trans 1,2,3,4-bis(isopropylidenedioxy)-cyclobutane (61845-71-4,110549-41-2) + exo-6,7-isopropylidenedioxy-1-methoxytricyclo<3.3.0.02.8>-oct-3-en (108805-95-4,108866-86-0) + endo-6,7-isopropylidenedioxy-1-methoxytricyclo<3.3.0.02.8>-oct-3-en (108805-95-4,108866-86-0) + exo-7,8-isopropylidenedioxy-1-methoxybicyclo<4.2.0>octa-2,4-diene (108805-96-5,108866-87-1) + endo-7,8-isopropylidenedioxy-1-methoxybicyclo<4.2.0>octa-2,4-diene (108805-96-5,108866-87-1)

Guidance literature:

In 1,4-dioxane; Product distribution; Irradiation; temperature dependence;

upstream raw materials:

2,2-dimethyl-[1,3]dioxole

methoxybenzene

benzonitrile

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