N-Cyclohexylphosphoramidothioic acid O,O-dimethyl ester

Base Information

• Chemical Name: N-Cyclohexylphosphoramidothioic acid O,O-dimethyl ester
• CAS No.: 941-39-9
• Molecular Formula: C8H18NO2PS
• Molecular Weight: 223.27
• Mol file: 941-39-9.mol

Synonyms:N-Cyclohexylphosphoramidothioic acid O,O-dimethyl ester

Chemical Property of N-Cyclohexylphosphoramidothioic acid O,O-dimethyl ester

Chemical Property:

• Melting Point: 90 - 91 °C
• PSA: 72.39000
• LogP: 3.46750

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Cyclohexylphosphoramidothioic acid O,O-dimethyl ester

There total 2 articles about N-Cyclohexylphosphoramidothioic acid O,O-dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

cyclohexylamine (108-91-8,157973-60-9) + dimethyl chlorothiophosphate (2524-03-0) → O,o'-dimethyl-N-cyclohexyl phosphoramido thionate (941-39-9)

Guidance literature:

With aluminum oxide; at 20 ℃;

DOI:10.1080/00304940709356016

Reference yield:

→ O,o'-dimethyl-N-cyclohexyl phosphoramido thionate (941-39-9)

Guidance literature:

Cyclohexylamin, Dimethylphosphorochloridothioat, CHCl3;

DOI:10.1039/jr9650002731

Reference yield:

O,o'-dimethyl-N-cyclohexyl phosphoramido thionate (941-39-9) + benzenesulfenyl chloride (931-59-9) → o,o'-dimethyl-N-phenylthio-N-cyclohexylphosphoramidothionate (53819-99-1)

Guidance literature:

With triethylamine; In cyclohexane;

upstream raw materials:

cyclohexylamine

dimethyl chlorothiophosphate

Downstream raw materials:

o,o'-dimethyl-N-phenylthio-N-cyclohexylphosphoramidothionate

O,O'-dimethyl-N-isopropylthio-N-cyclohexylphosphoramidothionate

Refernces