Technology Process of (6-bromopyridin-3-yl)(phenyl)methanamine
There total 5 articles about (6-bromopyridin-3-yl)(phenyl)methanamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; titanium tetrachloride;
In
1,2-dimethoxyethane;
at 0 - 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / 3 h / Reflux
2: aluminum (III) chloride / 6 h / Reflux
3: hydroxylamine hydrochloride; sodium carbonate / ethanol / 3 h / Reflux
4: sodium tetrahydroborate; titanium tetrachloride / 1,2-dimethoxyethane / 0 - 20 °C / Inert atmosphere
With
aluminum (III) chloride; sodium tetrahydroborate; thionyl chloride; hydroxylamine hydrochloride; titanium tetrachloride; sodium carbonate;
In
1,2-dimethoxyethane; ethanol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sodium carbonate / ethanol / 3 h / Reflux
2: sodium tetrahydroborate; titanium tetrachloride / 1,2-dimethoxyethane / 0 - 20 °C / Inert atmosphere
With
sodium tetrahydroborate; hydroxylamine hydrochloride; titanium tetrachloride; sodium carbonate;
In
1,2-dimethoxyethane; ethanol;
