2-Hydroxy-2-(4-methoxyphenyl)propionic acid

Base Information

• Chemical Name: 2-Hydroxy-2-(4-methoxyphenyl)propionic acid
• CAS No.: 91121-61-8
• Molecular Formula: C10H12O4
• Molecular Weight: 196.203
• Mol file: 91121-61-8.mol

Synonyms:2-Hydroxy-2-(4-methoxyphenyl)propionic acid;2-HYDROXY-2-(4-METHOXYPHENYL)PROPANOIC ACID;BENZENEACETIC ACID, A-HYDROXY-4-METHOXY-A-METHYL-

Chemical Property of 2-Hydroxy-2-(4-methoxyphenyl)propionic acid

Chemical Property:

• PSA: 66.76000
• LogP: 0.98730
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

2-Hydroxy-2-(4-methoxyphenyl)propanoicacid 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Hydroxy-2-(4-methoxyphenyl)propionic acid

There total 22 articles about 2-Hydroxy-2-(4-methoxyphenyl)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

p-methoxybenzoylformic acid (7099-91-4) + methyl iodide (74-88-4) → 2-(4-methoxyphenyl)-2-hydroxypropanoic acid (91121-61-8)

Guidance literature:

With magnesium; In tetrahydrofuran; diethyl ether;

Reference yield: 82.0%

carbon dioxide (124-38-9,18923-20-1) + 1-(4-methoxyphenyl)ethanone (100-06-1) → 2-(4-methoxyphenyl)-2-hydroxypropanoic acid (91121-61-8)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; In 1,2-dimethoxyethane; at 25 ℃; under 760 Torr; Electrochemical reaction;

DOI:10.1080/00397910500328811

Reference yield:

chloroform (67-66-3,8013-54-5) + 1-(4-methoxyphenyl)ethanone (100-06-1) → 2-(4-methoxyphenyl)-2-hydroxypropanoic acid (91121-61-8)

Guidance literature:

With potassium tert-butylate; In hexane; for 0.5h; Ambient temperature;

DOI:10.1016/S0040-4020(01)81926-8

upstream raw materials:

methyl magnesium iodide

p-methoxybenzoylformic acid

(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl (4-methoxyphenyl)(oxo)acetate

2-Oxo-propionic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Downstream raw materials:

2-(4-methoxy-phenyl)-acrylic acid

2-(4-methoxyphenyl)propanoic acid

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