Technology Process of 1-Isocyano-4-phenoxybenzene
There total 6 articles about 1-Isocyano-4-phenoxybenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; trichlorophosphate;
In
dichloromethane;
at 0 - 20 ℃;
for 24h;
DOI:10.1002/cmdc.201900472
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 12h;
Schlenk technique;
Inert atmosphere;
Sealed tube;
Green chemistry;
DOI:10.1021/acs.orglett.0c03472
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / dimethyl sulfoxide / 24 h / 100 °C / Sealed tube
2: hydrogen; palladium 10% on activated carbon / methanol / Inert atmosphere
3: toluene / 24 h / 110 °C / Sealed tube
4: triethylamine; trichlorophosphate / dichloromethane / 24 h / 0 - 20 °C
With
palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; trichlorophosphate;
In
methanol; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1002/cmdc.201900472
