methyl 2-(4-(ethylsulfonyl)phenyl)propanoate

Base Information

Chemical Name:methyl 2-(4-(ethylsulfonyl)phenyl)propanoate
CAS No.:1363179-18-3
Molecular Formula:C₁₂H₁₆O₄S
Molecular Weight:256.323
Hs Code.:
Mol file:1363179-18-3.mol

Synonyms:methyl 2-(4-(ethylsulfonyl)phenyl)propanoate

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Chemical Property of methyl 2-(4-(ethylsulfonyl)phenyl)propanoate

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Technology Process of methyl 2-(4-(ethylsulfonyl)phenyl)propanoate

There total 6 articles about methyl 2-(4-(ethylsulfonyl)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1363179-14-9
methyl [4-(ethylsulfonyl)phenyl]acetate

: 74-88-4
methyl iodide

: 1363179-18-3
methyl 2-[4-(ethylsulfonyl)phenyl]propanoate

Guidance literature:: methyl [4-(ethylsulfonyl)phenyl]acetate; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h; Sealed vial;

methyl iodide; In tetrahydrofuran; mineral oil; at 0 ℃; for 3h;

With hydrogenchloride; In tetrahydrofuran; water; mineral oil; pH=5;

Reference yield:

: ethyl 2-(4-(ethylsulfonyl)phenyl)acetate

: 1363179-18-3
methyl 2-[4-(ethylsulfonyl)phenyl]propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; water / ethanol / 20 °C

1.2: pH 1

2.1: thionyl chloride / 20 - 80 °C / Reflux

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Sealed vial

3.2: 3 h / 0 °C

3.3: pH 5

With thionyl chloride; water; sodium hydride; sodium hydroxide; In tetrahydrofuran; ethanol; mineral oil;

Reference yield:

: 1197-55-3
4-aminophenylacetic acid

: 1363179-18-3
methyl 2-[4-(ethylsulfonyl)phenyl]propanoate

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.75 h / 0 °C

1.2: 20 - 45 °C

2.1: potassium hydroxide; water / ethanol / 20 h / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 20 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

5.1: sodium hydroxide; water / ethanol / 20 °C

5.2: pH 1

6.1: thionyl chloride / 20 - 80 °C / Reflux

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Sealed vial

7.2: 3 h / 0 °C

7.3: pH 5

With hydrogenchloride; thionyl chloride; water; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; sodium hydroxide; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;