3-Bromo-5-chloro-2-methoxybenzaldehyde

Base Information

Chemical Name:3-Bromo-5-chloro-2-methoxybenzaldehyde
CAS No.:25299-26-7
Molecular Formula:C8H6BrClO2
Molecular Weight:249.491
Hs Code.:2913000090
DSSTox Substance ID:DTXSID70359592
Wikidata:Q82140869
Mol file:25299-26-7.mol

Synonyms:3-bromo-5-chloro-2-methoxybenzaldehyde;25299-26-7;SCHEMBL2389960;DTXSID70359592;MFCD05998291;AKOS000113733;BS-36611;CS-0116837;EN300-1725326;Z57635598

Suppliers and Price of 3-Bromo-5-chloro-2-methoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
3-bromo-5-chloro-2-methoxybenzaldehyde 95
10g
$ 2383.00

Labseeker
3-bromo-5-chloro-2-methoxybenzaldehyde 95
5g
$ 1467.00

ChemBridge Corporation
3-bromo-5-chloro-2-methoxybenzaldehyde 95%
200 μmol
$ 31.00

Total 6 raw suppliers

Chemical Property of 3-Bromo-5-chloro-2-methoxybenzaldehyde

Chemical Property:

Vapor Pressure:0.000668mmHg at 25°C
Melting Point:77 °C
Boiling Point:308.7°C at 760 mmHg
Flash Point:140.5°C
PSA：26.30000
Density:1.628g/cm³
LogP:2.92360
XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:247.92397
Heavy Atom Count:12
Complexity:165

Purity/Quality:

99% ^*data from raw suppliers

3-bromo-5-chloro-2-methoxybenzaldehyde 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1Br)Cl)C=O

Technology Process of 3-Bromo-5-chloro-2-methoxybenzaldehyde

There total 3 articles about 3-Bromo-5-chloro-2-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 19652-32-5
3-bromo-5-chlorosalicylaldehyde

: 74-88-4
methyl iodide

: 25299-26-7
3-bromo-5-chloro-2-(methyloxy)benzaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 14h;

Reference yield:

: 871339-17-2
[3-bromo-5-chloro-2-(methyloxy)phenyl]methanol

: 25299-26-7
3-bromo-5-chloro-2-(methyloxy)benzaldehyde

Guidance literature:: With sodium hypochlorite; sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; In dichloromethane; water; at 0 ℃; for 0.333333h;

Reference yield:

: 65851-97-0
methyl 3-bromo-5-chloro-2-methoxybenzoate

: 25299-26-7
3-bromo-5-chloro-2-(methyloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; lithium borohydride / tetrahydrofuran / 2 h / 50 °C

2: sodium hypochlorite; sodium hydrogencarbonate / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide / dichloromethane; water / 0.33 h / 0 °C

With methanol; sodium hypochlorite; lithium borohydride; sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; In tetrahydrofuran; dichloromethane; water;