Azetidine-1,3,3-tricarbox...

Base Information

• Chemical Name: Azetidine-1,3,3-tricarbox...
• CAS No.: 1011479-76-7
• Molecular Formula: C₁₂H₁₉NO₆
• Molecular Weight: 273.286
• Hs Code.: 2933998090
• Mol file: 1011479-76-7.mol

Synonyms:Azetidine-1,3,3-tricarbox...;Azetidine-1,3,3-tricarboxylic acid 1-tert-butyl ester 3-ethyl ester;1-[(tert-butoxy)carbonyl]-3-(ethoxycarbonyl)azetidine-3-carboxylic acid;1-Boc-3-ethoxycarbonylazetidine-3-carboxylic acid

Chemical Property of Azetidine-1,3,3-tricarbox...

Chemical Property:

• Boiling Point: 385.4±42.0 °C(Predicted)
• PKA: 2.32±0.20(Predicted)
• PSA: 93.14000
• Density: 1.276±0.06 g/cm3(Predicted)
• LogP: 0.80910

Purity/Quality:

97% ^*data from raw suppliers

Azetidine-1,3,3-tricarboxylicAcid1-tert-ButylEster3-EthylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Azetidine-1,3,3-tricarbox...

There total 1 articles about Azetidine-1,3,3-tricarbox... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(tert-butyl) 3,3-diethyl azetidine-1,3,3-tricarboxylate (1011479-75-6) → azetidine-1,3,3-tricarboxylic acid 1-tert-butyl ester 3-ethyl ester (1011479-76-7)

Guidance literature:

1-(tert-butyl) 3,3-diethyl azetidine-1,3,3-tricarboxylate; With sodium hydroxide; ethanol; water; for 39h;

With hydrogenchloride; water; In ethanol; pH=1;

Reference yield:

azetidine-1,3,3-tricarboxylic acid 1-tert-butyl ester 3-ethyl ester (1011479-76-7) + tert-butyl alcohol (75-65-0) → 3-tert-butoxycarbonylamino-azetidine-1,3-dicarboxylic acid 1-tert-butyl ester 3-ethyl ester (1105662-59-6)

Guidance literature:

azetidine-1,3,3-tricarboxylic acid 1-tert-butyl ester 3-ethyl ester; With diphenyl phosphoryl azide; triethylamine; In toluene; at 80 ℃; for 4h;

tert-butyl alcohol; In toluene; for 4h;

upstream raw materials:

1-(tert-butyl) 3,3-diethyl azetidine-1,3,3-tricarboxylate

Downstream raw materials:

3-tert-butoxycarbonylamino-azetidine-1,3-dicarboxylic acid 1-tert-butyl ester 3-ethyl ester

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