N-allyl-N-(1-(tert-butyldiphenylsilyloxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-allyl-N-(1-(tert-butyldiphenylsilyloxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide
CAS No.:1417743-30-6
Molecular Formula:C₃₁H₃₉NO₃SSi
Molecular Weight:533.807
Hs Code.:
Mol file:1417743-30-6.mol

Synonyms:N-allyl-N-(1-(tert-butyldiphenylsilyloxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

Suppliers and Price of N-allyl-N-(1-(tert-butyldiphenylsilyloxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-N-(1-(tert-butyldiphenylsilyloxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-allyl-N-(1-(tert-butyldiphenylsilyloxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

There total 4 articles about N-allyl-N-(1-(tert-butyldiphenylsilyloxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1417743-29-3
N-(1-((tert-butyldiphenylsilyl)oxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

: 106-95-6
allyl bromide

: 1417743-30-6
N-allyl-N-(1-((tert-butyldiphenylsilyl)oxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

: 304020-67-5
(2RS) 2-aminopent-4-en-1-ol

: 1417743-30-6
N-allyl-N-(1-((tert-butyldiphenylsilyl)oxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / water; ethyl acetate / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C

3: caesium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

With 1H-imidazole; sodium carbonate; caesium carbonate; In water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1069-48-3,7685-44-1
rac-allylglycine

: 1417743-30-6
N-allyl-N-(1-((tert-butyldiphenylsilyl)oxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C

2: sodium carbonate / water; ethyl acetate / 20 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C

4: caesium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; sodium carbonate; caesium carbonate; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide;