4-((tert-butyldiphenylsilyloxy)methyl)-3-aza-bicyclo[4.1.0]heptane

Base Information

Chemical Name:4-((tert-butyldiphenylsilyloxy)methyl)-3-aza-bicyclo[4.1.0]heptane
CAS No.:1417743-33-9
Molecular Formula:C₂₃H₃₁NOSi
Molecular Weight:365.591
Hs Code.:
Mol file:1417743-33-9.mol

Synonyms:4-((tert-butyldiphenylsilyloxy)methyl)-3-aza-bicyclo[4.1.0]heptane

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Chemical Property of 4-((tert-butyldiphenylsilyloxy)methyl)-3-aza-bicyclo[4.1.0]heptane

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Technology Process of 4-((tert-butyldiphenylsilyloxy)methyl)-3-aza-bicyclo[4.1.0]heptane

There total 4 articles about 4-((tert-butyldiphenylsilyloxy)methyl)-3-aza-bicyclo[4.1.0]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1417743-32-8
4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane

: 1417743-33-9
4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-azabicyclo[4.1.0]heptane

Guidance literature:: With ammonium chloride; magnesium; In methanol; at 23 ℃; Inert atmosphere;

Reference yield:

: 1417743-29-3
N-(1-((tert-butyldiphenylsilyl)oxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

: 1417743-33-9
4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-azabicyclo[4.1.0]heptane

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

2.1: Grubbs catalyst first generation / dichloromethane / 20 °C

3.1: diethylzinc; trifluoroacetic acid / hexane; dichloromethane / 0.33 h

3.2: 6 h / 20 °C

4.1: ammonium chloride; magnesium / methanol / 2 h / 23 °C / Inert atmosphere

With Grubbs catalyst first generation; diethylzinc; ammonium chloride; caesium carbonate; magnesium; trifluoroacetic acid; In methanol; hexane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1417743-30-6
N-allyl-N-(1-((tert-butyldiphenylsilyl)oxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

: 1417743-33-9
4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-azabicyclo[4.1.0]heptane

Guidance literature:: Multi-step reaction with 3 steps

1.1: Grubbs catalyst first generation / dichloromethane / 20 °C

2.1: diethylzinc; trifluoroacetic acid / hexane; dichloromethane / 0.33 h

2.2: 6 h / 20 °C

3.1: ammonium chloride; magnesium / methanol / 2 h / 23 °C / Inert atmosphere

With Grubbs catalyst first generation; diethylzinc; ammonium chloride; magnesium; trifluoroacetic acid; In methanol; hexane; dichloromethane;