4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane

Base Information

Chemical Name:4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane
CAS No.:1417743-32-8
Molecular Formula:C₃₀H₃₇NO₃SSi
Molecular Weight:519.78
Hs Code.:

Synonyms:4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane

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Chemical Property of 4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane

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Technology Process of 4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane

There total 4 articles about 4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-11-6
diiodomethane

: 1417743-31-7
2-(((tert-butyldiphenylsilyl)oxy)methyl)-1-tosyl-1,2,3,6-tetrahydropyridine

: 1417743-32-8
4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane

Guidance literature:: With diethylzinc; trifluoroacetic acid; In hexane; dichloromethane; at 20 ℃; for 6h; Cooling with ice;

Reference yield:

: 183247-69-0
N-(1-hydroxypent-4-en-2-yl)-4-methylbenzenesulfonamide

: 1417743-32-8
4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

3.1: Grubbs catalyst first generation / dichloromethane / 20 °C

4.1: diethylzinc; trifluoroacetic acid / hexane; dichloromethane / 0.33 h

4.2: 6 h / 20 °C

With 1H-imidazole; Grubbs catalyst first generation; diethylzinc; caesium carbonate; trifluoroacetic acid; In hexane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1417743-29-3
N-(1-((tert-butyldiphenylsilyl)oxy)pent-4-en-2-yl)-4-methylbenzenesulfonamide

: 1417743-32-8
4-(((tert-butyldiphenylsilyl)oxy)methyl)-3-tosyl-3-azabicyclo[4.1.0]heptane

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

2.1: Grubbs catalyst first generation / dichloromethane / 20 °C

3.1: diethylzinc; trifluoroacetic acid / hexane; dichloromethane / 0.33 h

3.2: 6 h / 20 °C

With Grubbs catalyst first generation; diethylzinc; caesium carbonate; trifluoroacetic acid; In hexane; dichloromethane; N,N-dimethyl-formamide;