tert-butyl 4-(3-methoxy-4-(2-methoxy-2-oxoethyl)phenoxy)piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-(3-methoxy-4-(2-methoxy-2-oxoethyl)phenoxy)piperidine-1-carboxylate
CAS No.:170930-04-8
Molecular Formula:C₂₀H₂₉NO₆
Molecular Weight:379.453
Hs Code.:
Mol file:170930-04-8.mol

Synonyms:tert-butyl 4-(3-methoxy-4-(2-methoxy-2-oxoethyl)phenoxy)piperidine-1-carboxylate

Suppliers and Price of tert-butyl 4-(3-methoxy-4-(2-methoxy-2-oxoethyl)phenoxy)piperidine-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 4-(3-methoxy-4-(2-methoxy-2-oxoethyl)phenoxy)piperidine-1-carboxylate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of tert-butyl 4-(3-methoxy-4-(2-methoxy-2-oxoethyl)phenoxy)piperidine-1-carboxylate

There total 5 articles about tert-butyl 4-(3-methoxy-4-(2-methoxy-2-oxoethyl)phenoxy)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36851-80-6
nitrosomethylurea

aqueous potassium hydroxide: aqueous potassium hydroxide

: 162045-85-4
2-methoxy-4-(1-Boc-4-piperidyloxy)benzoyl chloride

: 170930-04-8
methyl 2-methoxy-4-(1-Boc-4-piperidyloxy)-phenylacetate

Guidance literature:: silver benzoate; In tetrahydrofuran; methanol; dichloromethane; triethylamine;

Reference yield:

: 89-84-9
2',4'-dihydroxy-4-acetophenone

: 170930-04-8
methyl 2-methoxy-4-(1-Boc-4-piperidyloxy)-phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl azodicarboxylate, Ph₃P / tetrahydrofuran

2: Cs₂CO₃ / dimethylformamide

3: 1.) Tl(NO₃)3, 2.) Boc₂O, DIEA / 1.) MeOH, 2.) DMF

With di-tert-butyl dicarbonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; thallium(III) nitrate; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(99)00181-X

Reference yield:

: 109384-19-2
t-butyl 4-hydroxy piperidine-1-carboxylate

: 170930-04-8
methyl 2-methoxy-4-(1-Boc-4-piperidyloxy)-phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl azodicarboxylate, Ph₃P / tetrahydrofuran

2: Cs₂CO₃ / dimethylformamide

3: 1.) Tl(NO₃)3, 2.) Boc₂O, DIEA / 1.) MeOH, 2.) DMF

With di-tert-butyl dicarbonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; thallium(III) nitrate; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(99)00181-X