4-Chloro-2-(2,6-dichlorophenyl)-3H-iMidazo[4,5-c]pyridine

Base Information

• Chemical Name: 4-Chloro-2-(2,6-dichlorophenyl)-3H-iMidazo[4,5-c]pyridine
• CAS No.: 1334411-81-2
• Molecular Formula: C12H6Cl3N3
• Molecular Weight: 298.559
• Hs Code.: 2933990090
• Mol file: 1334411-81-2.mol

Synonyms:4-Chloro-2-(2,6-dichlorophenyl)-3H-iMidazo[4,5-c]pyridine

Chemical Property of 4-Chloro-2-(2,6-dichlorophenyl)-3H-iMidazo[4,5-c]pyridine

Chemical Property:

• Boiling Point: 517.1±60.0 °C(Predicted)
• PKA: 8.70±0.40(Predicted)
• PSA: 41.57000
• Density: 1.575±0.06 g/cm3(Predicted)
• LogP: 4.58510

Purity/Quality:

97% ^*data from raw suppliers

4-Chloro-2-(2,6-dichlorophenyl)-3H-imidazo[4,5-c]pyridine ^*data from reagent suppliers

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Technology Process of 4-Chloro-2-(2,6-dichlorophenyl)-3H-iMidazo[4,5-c]pyridine

There total 2 articles about 4-Chloro-2-(2,6-dichlorophenyl)-3H-iMidazo[4,5-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-chloropyridine-3,4-diamine (39217-08-8) + 2,6-Dichlorobenzoyl chloride (4659-45-4) → 4-chloro-2-(2,6-dichlorophenyl)-1H-imidazo[4,5-c]pyridine (1334411-81-2)

Guidance literature:

2-chloropyridine-3,4-diamine; 2,6-Dichlorobenzoyl chloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile; at 0 - 23 ℃;

With trichlorophosphate; at 120 ℃;

With sodium hydrogencarbonate; In water; pH=7;

Reference yield: 43.0%

2-chloropyridine-3,4-diamine (39217-08-8) + 2,6-dichlorobenzaldehyde (83-38-5) → 4-chloro-2-(2,6-dichlorophenyl)-1H-imidazo[4,5-c]pyridine (1334411-81-2)

Guidance literature:

With ammonium acetate; In ethanol; at 75 ℃; for 72h;

Reference yield: 70.0%

4-chloro-2-(2,6-dichlorophenyl)-1H-imidazo[4,5-c]pyridine (1334411-81-2) → 4-bromo-2-(2,6-dichlorophenyl)-1H-imidazo[4,5-c]pyridine (1334411-79-8)

Guidance literature:

4-chloro-2-(2,6-dichlorophenyl)-1H-imidazo[4,5-c]pyridine; With hydrogen bromide; acetic acid; at 90 ℃;

With potassium carbonate; In water; at 20 ℃; pH=7; Product distribution / selectivity; Cooling with ice;

upstream raw materials:

2-chloropyridine-3,4-diamine

2,6-Dichlorobenzoyl chloride

2,6-dichlorobenzaldehyde

Downstream raw materials:

C₁₃H₈BrCl₂N₃

C₁₃H₈BrCl₂N₃

4-bromo-2-(2,6-dichlorophenyl)-1H-imidazo[4,5-c]pyridine

2-(2,6-dichlorophenyl)-N-(pyridin-2-yl)-1H-imidazo[4,5-c]pyridin-4-amine

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