Technology Process of platinum(2+) potassium chloride ammoniate hydrate (1:1:3:1:1)
There total 7 articles about platinum(2+) potassium chloride ammoniate hydrate (1:1:3:1:1) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
AgNO3; KCl;
In
water;
(Pt(C2H5NH2)I2)2 was suspd. in water, AgNO3 was added, the mixt. was stirred at room temp. in the dark for 2 days, the ppt. AgI was filtered off and KCl was added to the filtrate, the mixt. was stirred for 24 h; the ppt. AgCl was removed, filtrate was evapd., the residue was dried in vac. for 24 h, dissolved in acetone and ppt.(KCl and KNO3) was filtered out, filtrate was evapd., residue dissolved in water, mixt. filtered, evapd., dried in vac.; X-ray diffract.;
- Guidance literature:
-
In
water;
byproducts: Pt; boiling of K2(PtCl4) in H2O with a 20% NH4-acetate-soln. for 1 1/2 h; filtration of Pt; pptn. with (Pt(NH3)4)Cl2; washing and drying of the (Pt(NH3)4)(Pt(NH3)Cl3)2-ppt.; trituration with K2(PtCl4) in an agate-bowl for 1-1 1/2 h;; extraction with a small amount of cold H2O; trituration and filtration of the mixture; evaporation; cooling down; sucking off;;
- Guidance literature:
-
With
potassium acetate;
In
ethanol;
