2-(3,5-DIMETHOXYBENZOYL)PYRIDINE

Base Information

• Chemical Name: 2-(3,5-DIMETHOXYBENZOYL)PYRIDINE
• CAS No.: 32864-08-7
• Molecular Formula: C14H13NO3
• Molecular Weight: 243.262
• Hs Code.: 2933399090
• Mol file: 32864-08-7.mol

Synonyms:2-(3,5-DIMETHOXYBENZOYL)PYRIDINE

Chemical Property of 2-(3,5-DIMETHOXYBENZOYL)PYRIDINE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 418.615°C at 760 mmHg
• PKA: 2.51±0.10(Predicted)
• Flash Point: 206.971°C
• PSA: 48.42000
• Density: 1.165g/cm³
• LogP: 2.32980

Purity/Quality:

97% ^*data from raw suppliers

2-(3,5-Dimethoxybenzoyl)pyridine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(3,5-DIMETHOXYBENZOYL)PYRIDINE

There total 3 articles about 2-(3,5-DIMETHOXYBENZOYL)PYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

2-iodopyridine (5029-67-4) + formic acid (64-18-6) + 3,5-dimethoxyphenylboronic acid (192182-54-0) → (3,5-dimethoxyphenyl)(pyridin-2-yl)methanone (32864-08-7)

Guidance literature:

With potassium carbonate; dicyclohexyl-carbodiimide; In toluene; at 100 ℃; for 12h; Inert atmosphere; Sealed tube;

DOI:10.1002/aoc.4650

Reference yield:

2-Cyanopyridine (100-70-9,1232006-36-8) + 1-bromo-3,5-dimethoxybenzene (20469-65-2) → (3,5-dimethoxyphenyl)(pyridin-2-yl)methanone (32864-08-7)

Guidance literature:

2-Cyanopyridine; 1-bromo-3,5-dimethoxybenzene; With magnesium; In tetrahydrofuran; at 0 ℃;

With ammonium chloride; In tetrahydrofuran;

DOI:10.1021/jo5027723

Reference yield:

→ (3,5-dimethoxyphenyl)(pyridin-2-yl)methanone (32864-08-7)

Guidance literature:

3,5-Dimethoxyphenyl-(2-pyridyl)-carbinol, Oxidation m. KMnO4;

upstream raw materials:

2-Cyanopyridine

1-bromo-3,5-dimethoxybenzene

2-iodopyridine

formic acid

Downstream raw materials:

3,5-Dimethoxyphenyl-(2-pyridyl)carbinol

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