1H-1,2,4-Triazole-5-carboxylic acid, 3-Methyl-1-(1-Methylethyl)-, ethyl ester

Base Information

Chemical Name:1H-1,2,4-Triazole-5-carboxylic acid, 3-Methyl-1-(1-Methylethyl)-, ethyl ester
CAS No.:1282517-47-8
Molecular Formula:C9H15N3O2
Molecular Weight:197.2343
Hs Code.:
Mol file:1282517-47-8.mol

Synonyms:1H-1,2,4-Triazole-5-carboxylic acid, 3-Methyl-1-(1-Methylethyl)-, ethyl ester

Suppliers and Price of 1H-1,2,4-Triazole-5-carboxylic acid, 3-Methyl-1-(1-Methylethyl)-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-methyl-1-(1-methylethyl)-1H-1,2,4-Triazole-5-carboxylicacidEthylEster
100mg
$ 350.00

ChemScene
1H-1,2,4-Triazole-5-carboxylicacid,3-methyl-1-(1-methylethyl)-,ethylester 99.16%
100mg
$ 190.00

AK Scientific
1H-1,2,4-Triazole-5-carboxylicacid,3-methyl-1-(1-methylethyl)-,ethylester
500mg
$ 678.80

Total 5 raw suppliers

Chemical Property of 1H-1,2,4-Triazole-5-carboxylic acid, 3-Methyl-1-(1-Methylethyl)-, ethyl ester

Chemical Property:

Boiling Point:320.3±25.0 °C(Predicted)
PKA:1.84±0.10(Predicted)
PSA：57.01000
Density:1.16±0.1 g/cm3(Predicted)
LogP:1.34410

Purity/Quality:

NLT 98% ^*data from raw suppliers

3-methyl-1-(1-methylethyl)-1H-1,2,4-Triazole-5-carboxylicacidEthylEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-1,2,4-Triazole-5-carboxylic acid, 3-Methyl-1-(1-Methylethyl)-, ethyl ester

There total 2 articles about 1H-1,2,4-Triazole-5-carboxylic acid, 3-Methyl-1-(1-Methylethyl)-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 4466-50-6
1-acetyl-2-isopropylhydrazine

: 16982-21-1
ethyl 2-amino-2-thioxoacetate

: 1282517-47-8
2-isopropyl-5-methyl-2H-[1,2,4]triazole-3-carboxylic acid ethyl ester

Guidance literature:: ethyl 2-amino-2-thioxoacetate; With trimethoxonium tetrafluoroborate; In dichloromethane; at 20 ℃; for 2h;

1-acetyl-2-isopropylhydrazine; With triethylamine; In dichloromethane; at 20 ℃; for 15h; Reflux;

Reference yield:

: 3742-63-0
acetic acid isopropylidenehydrazide

: 1282517-47-8
2-isopropyl-5-methyl-2H-[1,2,4]triazole-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen / platinum(IV) oxide / industrial methylated spirits / 48 h / 20 °C

2.1: trimethoxonium tetrafluoroborate / dichloromethane / 2 h / 20 °C

2.2: 15 h / 20 °C / Reflux

With hydrogen; trimethoxonium tetrafluoroborate; platinum(IV) oxide; In industrial methylated spirits; dichloromethane;

Reference yield: 75.0%

: 1282517-47-8
2-isopropyl-5-methyl-2H-[1,2,4]triazole-3-carboxylic acid ethyl ester

: 1282517-46-7
2-bromo-1-(2-isopropyl-5-methyl-2H-[1,2,4]triazol-3-yl)-ethanone

Guidance literature:: 2-isopropyl-5-methyl-2H-[1,2,4]triazole-3-carboxylic acid ethyl ester; With methyllithium; 1,1-dibromomethane; In formaldehyde diethyl acetal; at -78 ℃; for 0.25h;

With acetic acid; In tetrahydrofuran; formaldehyde diethyl acetal; at -78 - 20 ℃;