β-Bromobenzenepropionic acid methyl ester

Base Information

• Chemical Name: β-Bromobenzenepropionic acid methyl ester
• CAS No.: 16503-45-0
• Molecular Formula: C10H11BrO2
• Molecular Weight: 243.1
• Mol file: 16503-45-0.mol

Synonyms:β-Bromobenzenepropionic acid methyl ester;3-broMo-3-phenyl-propionic acid Methyl ester

Chemical Property of β-Bromobenzenepropionic acid methyl ester

Chemical Property:

• PSA: 26.30000
• LogP: 2.68570

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of β-Bromobenzenepropionic acid methyl ester

There total 18 articles about β-Bromobenzenepropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl 3-phenyl-3-(phenylthio)propanoate → methyl 3-bromo-3-phenylpropanoate (16503-45-0)

Guidance literature:

With bromine; In dichloromethane; at 20 ℃; for 0.416667h; Solvent; Temperature;

DOI:10.1039/c9sc03560e

Reference yield: 78.0%

1-methoxy-2-phenylcyclopropanol (56955-33-0) → methyl 3-bromo-3-phenylpropanoate (16503-45-0)

Guidance literature:

With bromine; Irradiation;

DOI:10.1016/S0040-4039(00)60864-X

Reference yield: 33.7%

methanol (67-56-1) → 1-(2-bromo-1-methoxyethyl)benzene (13685-00-2) + methyl 3-bromo-3-phenylpropanoate (16503-45-0) + methyl β-phenyl-β-methoxy-propionate (16510-80-8,42332-80-9,3461-35-6) + (1,2-dibromoethyl)benzene (102921-26-6,93-52-7)

Guidance literature:

With bromine; Further byproducts given;

DOI:10.1016/S0040-4039(00)92190-7

upstream raw materials:

methanol

3-bromo-3-phenylpropionic acid

methyl 3-hydroxy-3-phenylpropionate

1-methoxy-2-phenylcyclopropanol

Downstream raw materials:

Methyl-β-phenoxy-β-phenyl-propionat

meso-3,4-diphenyl-adipic acid dimethyl ester

dimethyl (3SR,4SR)-3,4-diphenylhexanedioate

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