3-Methyl-4-phenylcinnoline

Base Information

Chemical Name:3-Methyl-4-phenylcinnoline
CAS No.:21039-71-4
Molecular Formula:C15H12N2
Molecular Weight:220.274
Hs Code.:
Mol file:21039-71-4.mol

Synonyms:3-Methyl-4-phenylcinnoline

Suppliers and Price of 3-Methyl-4-phenylcinnoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Methyl-4-phenylcinnoline

Chemical Property:

PSA：25.78000
LogP:3.60520

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Methyl-4-phenylcinnoline

There total 6 articles about 3-Methyl-4-phenylcinnoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 412339-09-4
2-(1-phenylprop-1-en-1-yl)aniline

: 21039-71-4
3-methyl-4-phenylcinnoline

Guidance literature:: With tert.-butylnitrite; In ethanol; at 120 ℃; Inert atmosphere; Green chemistry;
DOI:10.1039/c7ob01553d

Reference yield:

: 673-32-5
1-Phenylprop-1-yne

: 265671-00-9
3,3-diethyl-1-(2-iodophenyl)triaz-1-ene

: 21039-71-4
3-methyl-4-phenylcinnoline

: 33732-51-3
4-methyl-3-phenylcinnoline

Guidance literature:: With tributyl-amine; tris-(o-tolyl)phosphine; palladium dichloride; In N,N-dimethyl-formamide; at 90 ℃; for 15h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.079

Reference yield:

: 6311-23-5
2-(toluene-4-sulfonylamino)-benzoic acid

: 21039-71-4
3-methyl-4-phenylcinnoline

Guidance literature:: Multi-step reaction with 4 steps

1: benzene; phosphorus pentachloride / Behandeln mit Aluminiumchlorid und Erwaermen des Produkts mit konz. Schwefelsaeure

2: diethyl ether

3: sulfuric acid

4: sodium nitrite; hydrochloric acid

With hydrogenchloride; diethyl ether; phosphorus pentachloride; sulfuric acid; sodium nitrite; benzene;