Tetramethyl 1,2,3,4-butanetetracarboxylate

Base Information

• Chemical Name: Tetramethyl 1,2,3,4-butanetetracarboxylate
• CAS No.: 24261-13-0
• Molecular Formula: C12H18O8
• Molecular Weight: 290.27
• Hs Code.: 2917190090
• Mol file: 24261-13-0.mol

Synonyms:Tetramethyl 1,2,3,4-butanetetracarboxylate;1,2,3,4-Butanetetracarboxylic acid tetramethyl ester

Chemical Property of Tetramethyl 1,2,3,4-butanetetracarboxylate

Chemical Property:

• PSA: 105.20000
• LogP: -0.30900

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tetramethyl 1,2,3,4-butanetetracarboxylate

There total 2 articles about Tetramethyl 1,2,3,4-butanetetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

methanol (67-56-1) + dimethyl cis-but-2-ene-1,4-dioate (624-48-6) + toluene (108-88-3,15644-74-3,16713-13-6) → methyl 5-oxotetrahydro-3-furancarboxylate (5204-91-1,681179-32-8) + tetramethyl 1,2,3,4-butanetetracarboxylate (24261-13-0) + dimethyl 2-benzylsuccinate (35262-43-2) + dimethyl 2-hydroxymethylsuccinate (50782-89-3)

Guidance literature:

With naphthalene-1,4-dicarbonitrile; In acetonitrile; tert-butyl alcohol; for 4h; Further byproducts given;

DOI:10.1002/(sici)1099-0690(199909)1999:9<2137::aid-ejoc2137>3.0.co;2-r

Reference yield:

dimethyl cis-but-2-ene-1,4-dioate (624-48-6) → tetramethyl 1,2,3,4-butanetetracarboxylate (24261-13-0) + Dimethyl succinate (106-65-0)

Guidance literature:

With sodium sulfide; triethylamine; cadmium(II) sulphide; In methanol; for 2h; Irradiation;

DOI:10.1039/ft9928801055

Reference yield: 75.0%

1,2,2,6,6-pentamethyl-piperidin-4-ol (2403-89-6) + tetramethyl 1,2,3,4-butanetetracarboxylate (24261-13-0) → tetrakis(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,2,3,4-butanetetracarboxylate

Guidance literature:

titanium(IV) isopropylate; In MSP; at 160 ℃; for 8h;

upstream raw materials:

dimethyl cis-but-2-ene-1,4-dioate

methanol

toluene

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