(2,3-Dihydrobenzofuran-6-yl)methanol

Base Information

Chemical Name:(2,3-Dihydrobenzofuran-6-yl)methanol
CAS No.:1083168-69-7
Molecular Formula:C9H10O2
Molecular Weight:150.177
Hs Code.:
DSSTox Substance ID:DTXSID30593071
Wikidata:Q82487472
Mol file:1083168-69-7.mol

Synonyms:(2,3-dihydrobenzofuran-6-yl)methanol;1083168-69-7;2,3-dihydro-1-benzofuran-6-ylmethanol;(2,3-Dihydro-1-benzofuran-6-yl)methanol;SCHEMBL3633962;DTXSID30593071;DLJJSKTZKULLGR-UHFFFAOYSA-N;MFCD18374755;AKOS015995275;DS-14814;DB-289695;CS-0060648;(2 pound not3-Dihydrobenzofuran-6-yl)methanol;Y10452;A895279;J-500568

Suppliers and Price of (2,3-Dihydrobenzofuran-6-yl)methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(2,3-Dihydrobenzofuran-6-yl)methanol
10mg
$ 45.00

Chemenu
(2,3-dihydrobenzofuran-6-yl)methanol 98%
1g
$ 587.00

Ambeed
(2,3-Dihydrobenzofuran-6-yl)methanol 98%
1g
$ 739.00

Ambeed
(2,3-Dihydrobenzofuran-6-yl)methanol 98%
100mg
$ 186.00

Ambeed
(2,3-Dihydrobenzofuran-6-yl)methanol 98%
250mg
$ 283.00

AK Scientific
2,3-dihydro-1-benzofuran-6-ylmethanol
1g
$ 1017.20

Abosyn
(2,3-dihydrobenzofuran-6-yl)methanol 98%
1g
$ 880.00

Abosyn
(2,3-dihydrobenzofuran-6-yl)methanol 98%
0.25g
$ 350.00

Abosyn
(2,3-dihydrobenzofuran-6-yl)methanol 98%
0.1g
$ 220.00

Total 14 raw suppliers

Chemical Property of (2,3-Dihydrobenzofuran-6-yl)methanol

Chemical Property:

PSA：29.46000
LogP:1.11380
Storage Temp.:2-8°C
XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:150.068079557
Heavy Atom Count:11
Complexity:136

Purity/Quality:

97% ^*data from raw suppliers

(2,3-Dihydrobenzofuran-6-yl)methanol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC2=C1C=CC(=C2)CO

Technology Process of (2,3-Dihydrobenzofuran-6-yl)methanol

There total 8 articles about (2,3-Dihydrobenzofuran-6-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1083168-68-6
methyl 2,3-dihydrobenzofuran-6-carboxylate

: 1083168-69-7
(2,3-dihydrobenzofuran-6-yl)methanol

Guidance literature:: methyl 2,3-dihydrobenzofuran-6-carboxylate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

With sodium hydroxide; water; In tetrahydrofuran;

Reference yield: 74.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 189035-22-1
6-bromo-2,3-dihydro-1-benzofuran

: 1083168-69-7
(2,3-dihydrobenzofuran-6-yl)methanol

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; pentane; at -74 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2015.05.047

Reference yield:

: 6272-26-0
6-hydroxybenzofuran-3-one

: 1083168-69-7
(2,3-dihydrobenzofuran-6-yl)methanol

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / dichloromethane / 3 h / 20 °C

2.1: sodium tetrahydroborate / methanol / 2 h / 20 °C

2.2: 3 h / 20 °C

3.1: pyridine / dichloromethane / 16 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / palladium diacetate; 1,3-bis-(diphenylphosphino)propane / N,N-dimethyl-formamide / 24 h / 70 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 2585.81 Torr

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

With pyridine; 1H-imidazole; sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen; N-ethyl-N,N-diisopropylamine; palladium diacetate; palladium 10% on activated carbon; 1,3-bis-(diphenylphosphino)propane; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;