5-Sulfo-1,3-benzenedicarboxylic acid, monolithium salt

Base Information

• Chemical Name: 5-Sulfo-1,3-benzenedicarboxylic acid, monolithium salt
• CAS No.: 46728-75-0
• Molecular Formula: C8H6 O7 S . Li
• Molecular Weight: 252.131
• Hs Code.: 29173995
• UNII: VV3666GGJQ
• Mol file: 46728-75-0.mol

Synonyms:VV3666GGJQ;LISIP;SCHEMBL673021;AKOS015894367;5-SULFO-1,3-BENZENEDICARBOXYLIC ACID, MONOLITHIUM SALT

Chemical Property of 5-Sulfo-1,3-benzenedicarboxylic acid, monolithium salt

Chemical Property:

• Melting Point: 300 ºC(lit.)
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 140.18000
• Density: g/cm³
• LogP: 1.06790
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 3
• Exact Mass: 251.99160210
• Heavy Atom Count: 17
• Complexity: 377

Purity/Quality:

97% ^*data from raw suppliers

5-Sulfoisophthalic acid monolithium salt ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 41-38
• Safety Statements: 26-36-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: [Li+].C1=C(C=C(C=C1C(=O)O)S(=O)(=O)[O-])C(=O)O
• Uses: Monomer for water-dispersible polyesters.

Technology Process of 5-Sulfo-1,3-benzenedicarboxylic acid, monolithium salt

There total 1 articles about 5-Sulfo-1,3-benzenedicarboxylic acid, monolithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-sulfoisophthalic acid (22326-31-4) → 5-sulfo-1,3-benzenedicarboxylic acid monolithium salt (46728-75-0)

Guidance literature:

With lithium hydroxide monohydrate; In water; at 0 - 110 ℃; Product distribution / selectivity;

Reference yield: 64.0%

5-sulfo-1,3-benzenedicarboxylic acid monolithium salt (46728-75-0) + copper(II) acetate monohydrate (6046-93-1) → Li24[Cu24(SO3-bdc)24]

Guidance literature:

for 1.5h; Milling;

DOI:10.1021/jacs.0c02806

Reference yield:

nickel(II) nitrate hexahydrate + 5-sulfo-1,3-benzenedicarboxylic acid monolithium salt (46728-75-0) + N,N-dimethyl-formamide (68-12-2,33513-42-7) + p-tert-butylsulfonylcalix[4]arene (204190-49-8) → {[Ni4(p-tert-butylsulfonylcalix[4]arene)(μ4-H2O)]4(5-sulfo-1,3-benzenedicarboxylate)8}[Ni(H2O)3(DMF)3]4(DMF)25(H2O)60

Guidance literature:

at 100 ℃; for 24h;

DOI:10.1039/c3cc47420h

upstream raw materials:

5-sulfoisophthalic acid