2-Oxetanecarboxylicacid,2-methyl-4-oxo-,methylester,(2S)-(9CI)

Base Information

Chemical Name:2-Oxetanecarboxylicacid,2-methyl-4-oxo-,methylester,(2S)-(9CI)
CAS No.:353302-31-5
Molecular Formula:C₆H₈O₄
Molecular Weight:144.127
Hs Code.:
Mol file:353302-31-5.mol

Synonyms:2-Oxetanecarboxylicacid,2-methyl-4-oxo-,methylester,(2S)-(9CI)

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Chemical Property of 2-Oxetanecarboxylicacid,2-methyl-4-oxo-,methylester,(2S)-(9CI)

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Technology Process of 2-Oxetanecarboxylicacid,2-methyl-4-oxo-,methylester,(2S)-(9CI)

There total 3 articles about 2-Oxetanecarboxylicacid,2-methyl-4-oxo-,methylester,(2S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 58653-97-7
methyl 2-methyl-2-oxiranecarboxylate

: 201230-82-2
carbon monoxide

: 353302-31-5
methyl 2-methyl-4-oxooxetane-2-carboxylate

Guidance literature:: With bis(tetrahydrofuran)-meso-tetraphenylporphyrinato aluminum tetracarbonyl cobaltate; In tetrahydrofuran; at 60 ℃; for 18h; under 46544.6 Torr; regioselective reaction;

Reference yield:

: 600-22-6
pyruvic acid methyl ester

: 4071-85-6
trimetylsilylketene

: 353302-31-5
(2S)-2-methyl-4-oxo-oxetane-2-carboxylic acid methyl ester

: 353302-31-5
(2R)-2-methyl-4-oxo-oxatane-2-carboxylic acid methyl ester

Guidance literature:: pyruvic acid methyl ester; trimetylsilylketene; [Cu((S,S)-((CH₃)3CCHCH₂OCN)2C(CH₃)2)](SbF₆)2; In dichloromethane; at -50 ℃; for 24h;

With potassium fluoride; In acetonitrile; at 20 ℃; for 0.333333h; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/ol016096z

Reference yield:

: 600-22-6
pyruvic acid methyl ester

: 4071-85-6
trimetylsilylketene

: 353302-31-5
(2S)-2-methyl-4-oxo-oxetane-2-carboxylic acid methyl ester

: 353302-31-5
(2R)-2-methyl-4-oxo-oxatane-2-carboxylic acid methyl ester

Guidance literature:: pyruvic acid methyl ester; trimetylsilylketene; [Cu((S,S)-((CH₃)3CCHCH₂OCN)2C(CH₃)2)](SbF₆)2; In dichloromethane; at -50 ℃; for 24h;

With potassium fluoride; In acetonitrile; at 20 ℃; for 0.333333h; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/ol016096z