Methyl 6-broMo-5-Methylnicotinate

Base Information

• Chemical Name: Methyl 6-broMo-5-Methylnicotinate
• CAS No.: 1210451-92-5
• Molecular Formula: C8H8BrNO2
• Molecular Weight: 230.05862
• Hs Code.: 2933399090
• Mol file: 1210451-92-5.mol

Synonyms:Methyl 6-broMo-5-Methylnicotinate

Chemical Property of Methyl 6-broMo-5-Methylnicotinate

Chemical Property:

• Boiling Point: 305.4±37.0 °C(Predicted)
• PKA: -0.95±0.20(Predicted)
• PSA: 39.19000
• Density: 1.503±0.06 g/cm3(Predicted)
• LogP: 1.93910
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Methyl6-bromo-5-methylnicotinate 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 6-broMo-5-Methylnicotinate

There total 2 articles about Methyl 6-broMo-5-Methylnicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-bromo-5-methylpyridine-3-carbaldehyde (885167-81-7) → Methyl 6-bromo-5-methylpyridine-3-carboxylate (1210451-92-5)

Guidance literature:

With N-iodo-succinimide; potassium carbonate; In methanol; at 20 ℃; for 3h; Darkness;

DOI:10.1002/anie.201101501

Reference yield:

methanol (67-56-1) + 6-bromo-5-methylpyridine-3-carbaldehyde (885167-81-7) → Methyl 6-bromo-5-methylpyridine-3-carboxylate (1210451-92-5)

Guidance literature:

With N-iodo-succinimide;

DOI:10.1002/anie.201004460

Reference yield:

Methyl 6-bromo-5-methylpyridine-3-carboxylate (1210451-92-5) → C8H7Br2NO2 (1260657-95-1)

Guidance literature:

With N-Bromosuccinimide; In tetrachloromethane;

DOI:10.1002/anie.201004460

upstream raw materials:

methanol

6-bromo-5-methylpyridine-3-carbaldehyde

Downstream raw materials:

C₈H₇Br₂NO₂

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