METHYL TRANS-2-HYDROXYMETHYLCYCLOHEXANE-1-CARBOXYLATE

Base Information

• Chemical Name: METHYL TRANS-2-HYDROXYMETHYLCYCLOHEXANE-1-CARBOXYLATE
• CAS No.: 71550-80-6
• Molecular Formula: C₉H₁₆O₃
• Molecular Weight: 172.224
• Hs Code.: 2918199090
• Mol file: 71550-80-6.mol

Synonyms:METHYL TRANS-2-HYDROXYMETHYLCYCLOHEXANE-1-CARBOXYLATE

Chemical Property of METHYL TRANS-2-HYDROXYMETHYLCYCLOHEXANE-1-CARBOXYLATE

Chemical Property:

• Vapor Pressure: 0.00338mmHg at 25°C
• Boiling Point: 250.7°C at 760 mmHg
• Flash Point: 99.8°C
• PSA: 46.53000
• Density: 1.058g/cm³
• LogP: 0.95810

Purity/Quality:

97% ^*data from raw suppliers

Methyltrans-2-hydroxymethylcyclohexane-1-carboxylate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYL TRANS-2-HYDROXYMETHYLCYCLOHEXANE-1-CARBOXYLATE

There total 7 articles about METHYL TRANS-2-HYDROXYMETHYLCYCLOHEXANE-1-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-1,2-cyclohexanedicarboxylic acid,monomethyl ester (7719-08-6) → 2-hydroxymethyl-cyclohexanecarboxylic acid methyl ester (71550-80-6,96894-63-2,116261-06-4)

Guidance literature:

With borane; In tetrahydrofuran; water;

Reference yield:

2-benzofuran-1(3H)-one (87-41-2) → 2-hydroxymethyl-cyclohexanecarboxylic acid methyl ester (71550-80-6,96894-63-2,116261-06-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium; isoamyl alcohol

2: concentrated sulfuric acid

With i-Amyl alcohol; sulfuric acid; sodium;

Reference yield:

2-(chloromethyl)benzamide (13169-51-2) → 2-hydroxymethyl-cyclohexanecarboxylic acid methyl ester (71550-80-6,96894-63-2,116261-06-4)

Guidance literature:

Multi-step reaction with 4 steps

2: concentrated hydrochloric acid

3: sodium; amyl alcohol

4: concentrated sulfuric acid

With hydrogenchloride; pentan-1-ol; sulfuric acid; sodium;

upstream raw materials:

methanol

2-hydroxymethyl-cyclohexanecarboxylic acid

2-benzofuran-1(3H)-one

2-(chloromethyl)benzamide